ethyl N-(2-acetamido-3,4,6-tri-O-acetyl-2-deoxy-β-D-glucopyranosyl)benzylphosphonamide

Base Information

Chemical Name:ethyl N-(2-acetamido-3,4,6-tri-O-acetyl-2-deoxy-β-D-glucopyranosyl)benzylphosphonamide
CAS No.:211516-69-7
Molecular Formula:C₂₃H₃₃N₂O₁₀P
Molecular Weight:528.496
Hs Code.:

Synonyms:ethyl N-(2-acetamido-3,4,6-tri-O-acetyl-2-deoxy-β-D-glucopyranosyl)benzylphosphonamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of ethyl N-(2-acetamido-3,4,6-tri-O-acetyl-2-deoxy-β-D-glucopyranosyl)benzylphosphonamide

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Technology Process of ethyl N-(2-acetamido-3,4,6-tri-O-acetyl-2-deoxy-β-D-glucopyranosyl)benzylphosphonamide

There total 2 articles about ethyl N-(2-acetamido-3,4,6-tri-O-acetyl-2-deoxy-β-D-glucopyranosyl)benzylphosphonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 45.0%

: 4515-24-6
2-acetamido-2-deoxy-3,4,6-tri-O-acetyl-β-D-glucopyranosylamine

: 41760-95-6
monoethyl P-benzylphosphonochloridate

: 211516-69-7
ethyl N-(2-acetamido-3,4,6-tri-O-acetyl-2-deoxy-β-D-glucopyranosyl)benzylphosphonamide

Guidance literature:: With pyridine; In dichloromethane; at 0 - 20 ℃; for 17h;
DOI:10.1139/cjc-76-3-313

Reference yield:

: 6205-69-2
2-acetamido-3,4,6-tri-O-acetyl-2-deoxy-β-D-glucopyranosyl azide

: 211516-69-7
ethyl N-(2-acetamido-3,4,6-tri-O-acetyl-2-deoxy-β-D-glucopyranosyl)benzylphosphonamide

Guidance literature:: Multi-step reaction with 2 steps

1: H₂ / PtO₂ / ethanol / 5 h / Ambient temperature

2: 45 percent / pyridine / CH₂Cl₂ / 17 h / 0 - 20 °C

With pyridine; hydrogen; platinum(IV) oxide; In ethanol; dichloromethane;
DOI:10.1139/cjc-76-3-313