3-{[6-(3,4-dichlorophenyl)pyrimidin-4-yl]hydrazono}butyric acid ethyl ester

Base Information

Chemical Name:3-{[6-(3,4-dichlorophenyl)pyrimidin-4-yl]hydrazono}butyric acid ethyl ester
CAS No.:1319158-58-1
Molecular Formula:C₁₆H₁₆Cl₂N₄O₂
Molecular Weight:367.235
Hs Code.:

Synonyms:3-{[6-(3,4-dichlorophenyl)pyrimidin-4-yl]hydrazono}butyric acid ethyl ester

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Chemical Property of 3-{[6-(3,4-dichlorophenyl)pyrimidin-4-yl]hydrazono}butyric acid ethyl ester

Chemical Property:

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Technology Process of 3-{[6-(3,4-dichlorophenyl)pyrimidin-4-yl]hydrazono}butyric acid ethyl ester

There total 4 articles about 3-{[6-(3,4-dichlorophenyl)pyrimidin-4-yl]hydrazono}butyric acid ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1319158-56-9
[6-(3,4-dichlorophenyl)pyrimidin-4-yl]hydrazine

: 141-97-9
ethyl acetoacetate

: 1319158-58-1
3-{[6-(3,4-dichlorophenyl)pyrimidin-4-yl]hydrazono}butyric acid ethyl ester

Guidance literature:: In ethanol; for 2h; Reflux;

Reference yield:

: 954224-40-9
4-chloro-6-(3,4-dichloro-phenyl)-pyrimidine

: 1319158-58-1
3-{[6-(3,4-dichlorophenyl)pyrimidin-4-yl]hydrazono}butyric acid ethyl ester

Guidance literature:: Multi-step reaction with 3 steps

1.1: 1,4-dioxane / 6 h / Inert atmosphere; Reflux

2.1: hydrogenchloride / 1,4-dioxane; methanol / 4 h / 20 °C

2.2: 1 h / 20 °C

3.1: ethanol / 2 h / Reflux

With hydrogenchloride; In 1,4-dioxane; methanol; ethanol;

Reference yield:

: 1319158-53-6
N'-[6-(3,4-dichlorophenyl)pyrimidin-4-yl]hydrazinecarboxylic acid tert-butyl ester

: 1319158-58-1
3-{[6-(3,4-dichlorophenyl)pyrimidin-4-yl]hydrazono}butyric acid ethyl ester

Guidance literature:: Multi-step reaction with 2 steps

1.1: hydrogenchloride / 1,4-dioxane; methanol / 4 h / 20 °C

1.2: 1 h / 20 °C

2.1: ethanol / 2 h / Reflux

With hydrogenchloride; In 1,4-dioxane; methanol; ethanol;