1-benzyl 4-(2-( piperidin-1-yl)ethyl)piperazine-1,4-bis(carbodithioate)

Base Information

Chemical Name:1-benzyl 4-(2-( piperidin-1-yl)ethyl)piperazine-1,4-bis(carbodithioate)
CAS No.:1605349-76-5
Molecular Formula:C₂₀H₂₉N₃S₄
Molecular Weight:439.734
Hs Code.:

Synonyms:1-benzyl 4-(2-( piperidin-1-yl)ethyl)piperazine-1,4-bis(carbodithioate)

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Chemical Property of 1-benzyl 4-(2-( piperidin-1-yl)ethyl)piperazine-1,4-bis(carbodithioate)

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Technology Process of 1-benzyl 4-(2-( piperidin-1-yl)ethyl)piperazine-1,4-bis(carbodithioate)

There total 4 articles about 1-benzyl 4-(2-( piperidin-1-yl)ethyl)piperazine-1,4-bis(carbodithioate) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 49.7%

: 1932-03-2
2-(piperidin-4-yl)ethyl chloride

: 1605349-68-5
sodium 4-(benzylthiocarbonothioyl)piperazine-1-carbodithioate

: 1605349-71-0
benzyl 4-(2-(piperidin-1-yl)ethyl) piperazine-1-carbodithioate

: 1605349-76-5
1-benzyl 4-(2-( piperidin-1-yl)ethyl)piperazine-1,4-bis(carbodithioate)

Guidance literature:: With triethylamine; In methanol; at 20 ℃; for 3h;
DOI:10.1039/c4ob00005f

Reference yield:

: 139160-74-0
sodium 4-(tert-butoxycarbonyl)piperazine-1-carbodithioate

: 1605349-71-0
benzyl 4-(2-(piperidin-1-yl)ethyl) piperazine-1-carbodithioate

: 1605349-76-5
1-benzyl 4-(2-( piperidin-1-yl)ethyl)piperazine-1,4-bis(carbodithioate)

Guidance literature:: Multi-step reaction with 4 steps

1.1: triethylamine / methanol / 3 h / 20 °C

2.1: trifluoroacetic acid / dichloromethane / 6 h / 0 - 20 °C

2.2: 4 h / 0 - 20 °C

3.1: sodium hydroxide / ethyl acetate; water / 10 h / 5 - 20 °C

4.1: triethylamine / methanol / 3 h / 20 °C

With triethylamine; trifluoroacetic acid; sodium hydroxide; In methanol; dichloromethane; water; ethyl acetate;
DOI:10.1039/c4ob00005f

Reference yield:

: 1605349-59-4
tert-butyl 4-(benzylthiocarbonothioyl)piperazine-1-carboxylate

: 1605349-71-0
benzyl 4-(2-(piperidin-1-yl)ethyl) piperazine-1-carbodithioate

: 1605349-76-5
1-benzyl 4-(2-( piperidin-1-yl)ethyl)piperazine-1,4-bis(carbodithioate)

Guidance literature:: Multi-step reaction with 3 steps

1.1: trifluoroacetic acid / dichloromethane / 6 h / 0 - 20 °C

1.2: 4 h / 0 - 20 °C

2.1: sodium hydroxide / ethyl acetate; water / 10 h / 5 - 20 °C

3.1: triethylamine / methanol / 3 h / 20 °C

With triethylamine; trifluoroacetic acid; sodium hydroxide; In methanol; dichloromethane; water; ethyl acetate;
DOI:10.1039/c4ob00005f