Technology Process of C24H12BrClF2N2OS
There total 6 articles about C24H12BrClF2N2OS which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
2,3-dicyano-5,6-dichloro-p-benzoquinone;
In
toluene;
for 3h;
Reflux;
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: catacxium A; palladium diacetate; caesium carbonate / water; toluene / 16 h / 100 °C / Inert atmosphere
2.1: n-butyllithium / tetrahydrofuran / 2 h / -78 °C / Inert atmosphere
2.2: 1 h / -78 - 25 °C
3.1: trifluoroacetic acid / acetonitrile / 1 h / 25 °C
4.1: 2,3-dicyano-5,6-dichloro-p-benzoquinone / toluene / 3 h / Reflux
With
n-butyllithium; palladium diacetate; caesium carbonate; trifluoroacetic acid; 2,3-dicyano-5,6-dichloro-p-benzoquinone; catacxium A;
In
tetrahydrofuran; water; toluene; acetonitrile;
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: n-butyllithium / tetrahydrofuran / 2 h / -78 °C / Inert atmosphere
1.2: 1 h / -78 - 25 °C
2.1: trifluoroacetic acid / acetonitrile / 1 h / 25 °C
3.1: 2,3-dicyano-5,6-dichloro-p-benzoquinone / toluene / 3 h / Reflux
With
n-butyllithium; trifluoroacetic acid; 2,3-dicyano-5,6-dichloro-p-benzoquinone;
In
tetrahydrofuran; toluene; acetonitrile;