{(4R,5S)-5-[2-(tert-Butyl-diphenyl-silanyloxy)-ethyl]-2,2-dimethyl-[1,3]dioxolan-4-yl}-methanol

Base Information

Chemical Name:{(4R,5S)-5-[2-(tert-Butyl-diphenyl-silanyloxy)-ethyl]-2,2-dimethyl-[1,3]dioxolan-4-yl}-methanol
CAS No.:791101-25-2
Molecular Formula:C₂₄H₃₄O₄Si
Molecular Weight:414.617
Hs Code.:

Synonyms:{(4R,5S)-5-[2-(tert-Butyl-diphenyl-silanyloxy)-ethyl]-2,2-dimethyl-[1,3]dioxolan-4-yl}-methanol

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Chemical Property of {(4R,5S)-5-[2-(tert-Butyl-diphenyl-silanyloxy)-ethyl]-2,2-dimethyl-[1,3]dioxolan-4-yl}-methanol

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Technology Process of {(4R,5S)-5-[2-(tert-Butyl-diphenyl-silanyloxy)-ethyl]-2,2-dimethyl-[1,3]dioxolan-4-yl}-methanol

There total 3 articles about {(4R,5S)-5-[2-(tert-Butyl-diphenyl-silanyloxy)-ethyl]-2,2-dimethyl-[1,3]dioxolan-4-yl}-methanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 66.0%

: 84608-35-5
2-((4S,5R)-5-Hydroxymethyl-2,2-dimethyl-[1,3]dioxolan-4-yl)-ethanol

: 58479-61-1
tert-butylchlorodiphenylsilane

: 791101-25-2
{(4R,5S)-5-[2-(tert-Butyl-diphenyl-silanyloxy)-ethyl]-2,2-dimethyl-[1,3]dioxolan-4-yl}-methanol

Guidance literature:: 2-((4S,5R)-5-Hydroxymethyl-2,2-dimethyl-[1,3]dioxolan-4-yl)-ethanol; With 1H-imidazole; In N,N-dimethyl-formamide; at 23 ℃; for 0.25h; Inert atmosphere;

tert-butylchlorodiphenylsilane; In N,N-dimethyl-formamide; at 23 ℃; for 2h; Inert atmosphere;
DOI:10.1002/chem.200901375

Reference yield: 66.0%

: 84608-35-5
2-((4S,5R)-5-Hydroxymethyl-2,2-dimethyl-[1,3]dioxolan-4-yl)-ethanol

: 58479-61-1
tert-butylchlorodiphenylsilane

: 791101-25-2
{(4R,5S)-5-[2-(tert-Butyl-diphenyl-silanyloxy)-ethyl]-2,2-dimethyl-[1,3]dioxolan-4-yl}-methanol

: 2-((4S,5R)-5-(((tert-butyldiphenylsilyl)oxy)methyl)-2,2-dimethyl-1,3-dioxolan-4-yl)ethan-1-ol

Guidance literature:: With 1H-imidazole; In N,N-dimethyl-formamide; at 23 ℃; for 2h;
DOI:10.1002/anie.200702406

Reference yield:

: 791101-24-1
C₂₉H₄₂O₅Si

: 791101-25-2
{(4R,5S)-5-[2-(tert-Butyl-diphenyl-silanyloxy)-ethyl]-2,2-dimethyl-[1,3]dioxolan-4-yl}-methanol

Guidance literature:: C₂₉H₄₂O₅Si; With lithium aluminium tetrahydride; In tetrahydrofuran; at 0 ℃; for 0.166667h;

With sodium hydroxide; water; In tetrahydrofuran;