Technology Process of 4-(3,4-dimethoxyphenyl)-2-methylpiperidine
There total 5 articles about 4-(3,4-dimethoxyphenyl)-2-methylpiperidine which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
hydrogen;
palladium 10% on activated carbon; acetic acid;
In
methanol;
for 18h;
- Guidance literature:
-
Multi-step reaction with 2 steps
1: sodium tetrahydroborate; methanol / 17 h / 0 - 20 °C
2: hydrogen / acetic acid; palladium 10% on activated carbon / methanol / 18 h
With
methanol; sodium tetrahydroborate; hydrogen;
palladium 10% on activated carbon; acetic acid;
In
methanol;
- Guidance literature:
-
Multi-step reaction with 4 steps
1: potassium phosphate / 1,3-bis-(diphenylphosphino)propane; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride / toluene; water / 20 h / Reflux
2: acetone / 48 h
3: sodium tetrahydroborate; methanol / 17 h / 0 - 20 °C
4: hydrogen / acetic acid; palladium 10% on activated carbon / methanol / 18 h
With
methanol; sodium tetrahydroborate; potassium phosphate; hydrogen;
(1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; palladium 10% on activated carbon; 1,3-bis-(diphenylphosphino)propane; acetic acid;
In
methanol; water; acetone; toluene;
