(3S,4R)-(-)-4-(tert-butyldiphenylsilyloxy)-6-methoxy-3-phenyl-3,4-dihydroisoquinoline

Base Information

Chemical Name:(3S,4R)-(-)-4-(tert-butyldiphenylsilyloxy)-6-methoxy-3-phenyl-3,4-dihydroisoquinoline
CAS No.:158666-74-1
Molecular Formula:C₃₂H₃₃NO₂Si
Molecular Weight:491.705
Hs Code.:

Synonyms:(3S,4R)-(-)-4-(tert-butyldiphenylsilyloxy)-6-methoxy-3-phenyl-3,4-dihydroisoquinoline

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (3S,4R)-(-)-4-(tert-butyldiphenylsilyloxy)-6-methoxy-3-phenyl-3,4-dihydroisoquinoline

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Technology Process of (3S,4R)-(-)-4-(tert-butyldiphenylsilyloxy)-6-methoxy-3-phenyl-3,4-dihydroisoquinoline

There total 2 articles about (3S,4R)-(-)-4-(tert-butyldiphenylsilyloxy)-6-methoxy-3-phenyl-3,4-dihydroisoquinoline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 158666-73-0
(1'S,2'R)-(-)-N-<2-(tert-butyldiphenylsilyloxy)-2-(3-methoxyphenyl)-1-phenylethyl>formamide

: 158666-74-1
(3S,4R)-(-)-4-(tert-butyldiphenylsilyloxy)-6-methoxy-3-phenyl-3,4-dihydroisoquinoline

Guidance literature:: With phosphorus pentachloride; In dichloromethane; for 3h; Ambient temperature;
DOI:10.1016/0957-4166(94)80127-4

Reference yield:

: (1S,2R)-(-)-2-(tert-butyldiphenylsilyloxy)-2-(3-methoxyphenyl)-phenylethylamine hydrochloride

: 158666-74-1
(3S,4R)-(-)-4-(tert-butyldiphenylsilyloxy)-6-methoxy-3-phenyl-3,4-dihydroisoquinoline

Guidance literature:: Multi-step reaction with 2 steps

1: 94 percent / 0.33 h / 150 °C

2: 96 percent / PCl₅ / CH₂Cl₂ / 3 h / Ambient temperature

With phosphorus pentachloride; In dichloromethane;
DOI:10.1016/0957-4166(94)80127-4