C₂₉H₂₆O₄

Base Information

Chemical Name:C₂₉H₂₆O₄
CAS No.:1350895-95-2
Molecular Formula:C₂₉H₂₆O₄
Molecular Weight:438.523
Hs Code.:

C<sub>29</sub>H<sub>26</sub>O<sub>4</sub>

Synonyms:C₂₉H₂₆O₄

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Chemical Property of C₂₉H₂₆O₄

Chemical Property:

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Technology Process of C₂₉H₂₆O₄

There total 12 articles about C₂₉H₂₆O₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₃₀H₂₇BrO₅

: 1350895-94-1
(2R,3R)-2-phenyl-5,7-dibenzyloxy-chroman-3-ol

: 1350895-95-2
C₂₉H₂₆O₄

: C₂₉H₂₆O₄

Guidance literature:: C₃₀H₂₇BrO₅; With potassium carbonate; In acetone; at 20 ℃; for 48h; Inert atmosphere;

With sodium tetrahydroborate; In methanol; 1,2-dimethoxyethane; at 20 ℃; for 1.25h; Inert atmosphere;
DOI:10.1016/j.bmcl.2011.09.116

Reference yield:

: 1350896-05-7
C₃₁H₃₁BrO₄

: 1350895-94-1
(2R,3R)-2-phenyl-5,7-dibenzyloxy-chroman-3-ol

: 1350895-95-2
C₂₉H₂₆O₄

: C₂₉H₂₆O₄

Guidance literature:: Multi-step reaction with 6 steps

1.1: 1,8-diazabicyclo[5.4.0]undec-7-ene / toluene / 24 h / 110 °C / Inert atmosphere

2.1: AD-mix β; methanesulfonamide / tetrahydrofuran; water; tert-butyl alcohol / 120 h / 0 °C

3.1: hydrogenchloride / methanol; diethyl ether; water / 6.5 h / Reflux; Inert atmosphere

4.1: pyridinium p-toluenesulfonate / dichloromethane / 1 h / 20 °C / Inert atmosphere

5.1: dichloromethane / 1.17 h / 0 °C / Inert atmosphere; Molecular sieve

6.1: potassium carbonate / acetone / 48 h / 20 °C / Inert atmosphere

6.2: 1.25 h / 20 °C / Inert atmosphere

With hydrogenchloride; methanesulfonamide; AD-mix β; pyridinium p-toluenesulfonate; potassium carbonate; 1,8-diazabicyclo[5.4.0]undec-7-ene; In tetrahydrofuran; methanol; diethyl ether; dichloromethane; water; acetone; toluene; tert-butyl alcohol; 2.1: Sharpless dihydroxylation;
DOI:10.1016/j.bmcl.2011.09.116

Reference yield:

: C₃₁H₃₂O₆

: 1350895-94-1
(2R,3R)-2-phenyl-5,7-dibenzyloxy-chroman-3-ol

: 1350895-95-2
C₂₉H₂₆O₄

: C₂₉H₂₆O₄

Guidance literature:: Multi-step reaction with 5 steps

1.1: diethyl ether; ethyl acetate

2.1: hydrogenchloride / methanol; diethyl ether; water / 6.5 h / Reflux; Inert atmosphere

3.1: pyridinium p-toluenesulfonate / dichloromethane / 1 h / 20 °C / Inert atmosphere

4.1: dichloromethane / 1.17 h / 0 °C / Inert atmosphere; Molecular sieve

5.1: potassium carbonate / acetone / 48 h / 20 °C / Inert atmosphere

5.2: 1.25 h / 20 °C / Inert atmosphere

With hydrogenchloride; pyridinium p-toluenesulfonate; potassium carbonate; In methanol; diethyl ether; dichloromethane; water; ethyl acetate; acetone;
DOI:10.1016/j.bmcl.2011.09.116