tosylate de cyclopropylidene-3 propanol

Base Information

• Chemical Name: tosylate de cyclopropylidene-3 propanol
• CAS No.: 72064-31-4
• Molecular Formula: C₁₃H₁₆O₃S
• Molecular Weight: 252.334
• Mol file: 72064-31-4.mol

Synonyms:tosylate de cyclopropylidene-3 propanol

Chemical Property of tosylate de cyclopropylidene-3 propanol

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of tosylate de cyclopropylidene-3 propanol

There total 2 articles about tosylate de cyclopropylidene-3 propanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

diazomethane (186581-53-3,908094-01-9,334-88-3) + 3,4-pentadien-1-ol tosylate (24767-71-3) → tosylate de cyclopropylidene-3 propanol (72064-31-4)

Guidance literature:

With palladium diacetate; for 2h; Product distribution; other reaction time: 0.5 h.;

Reference yield:

→ tosylate de cyclopropylidene-3 propanol (72064-31-4)

Guidance literature:

entspr. Alkohol (4a);

Reference yield: 40.0%

(S)-1-phenyl-ethylamine (2627-86-3) + tosylate de cyclopropylidene-3 propanol (72064-31-4) → (S)-3-cyclopropylidene-N-(1-phenylethyl)propan-1-amine (506420-44-6)

Guidance literature:

With potassium carbonate; sodium iodide; In N,N-dimethyl-formamide; at 100 ℃;

DOI:10.1021/jo026535n

upstream raw materials:

diazomethane

3,4-pentadien-1-ol tosylate

Downstream raw materials:

hydroxy-1 cyclopropyl-1 cyclopropane

cyclopropyl-2 propene-2 ol-1

1-hydroxy-3-cyclopropylidenepropane

(S)-3-cyclopropylidene-N-(1-phenylethyl)propan-1-amine