C₂₇H₄₂O₈

Base Information

Chemical Name:C₂₇H₄₂O₈
CAS No.:1365268-24-1
Molecular Formula:C₂₇H₄₂O₈
Molecular Weight:494.626
Hs Code.:

C<sub>27</sub>H<sub>42</sub>O<sub>8</sub>

Synonyms:C₂₇H₄₂O₈

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Chemical Property of C₂₇H₄₂O₈

Chemical Property:

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Technology Process of C₂₇H₄₂O₈

There total 12 articles about C₂₇H₄₂O₈ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: 1365268-50-3
C₂₈H₄₄O₈

: 1365268-24-1
C₂₇H₄₂O₈

Guidance literature:: With pig liver esterase; water; In dimethyl sulfoxide; at 30 ℃; for 17h; pH=8; aq. phosphate buffer; Enzymatic reaction;
DOI:10.1016/j.tetlet.2012.01.058

Reference yield:

: C₁₉H₂₄O₂

: 1365268-24-1
C₂₇H₄₂O₈

Guidance literature:: Multi-step reaction with 12 steps

1.1: toluene-4-sulfonic acid / benzene / Reflux

2.1: n-butyllithium / tetrahydrofuran / -78 °C

2.2: -78 - 20 °C

3.1: sodium bis(2-methoxyethoxy)aluminium dihydride / diethyl ether / 20 °C

3.2: 0 °C

3.3: -78 °C

4.1: 1H-imidazole / dichloromethane / 20 °C

5.1: tetrakis(triphenylphosphine) palladium⁽⁰⁾; triethylamine / 60 °C

6.1: diisobutylaluminium hydride / dichloromethane / -78 °C

7.1: hydrogenchloride; water / tetrahydrofuran / 20 °C

8.1: N-ethyl-N,N-diisopropylamine / 1,2-dichloro-ethane / 50 °C

9.1: lithium diisopropyl amide / tetrahydrofuran / -78 °C

9.2: -78 °C

10.1: N-ethyl-N,N-diisopropylamine / 1,2-dichloro-ethane / 50 °C

11.1: pyridine hydrofluoride / tetrahydrofuran / 0 °C

12.1: pig liver esterase; water / dimethyl sulfoxide / 17 h / 30 °C / pH 8 / aq. phosphate buffer; Enzymatic reaction

With 1H-imidazole; hydrogenchloride; tetrakis(triphenylphosphine) palladium⁽⁰⁾; n-butyllithium; pig liver esterase; pyridine hydrofluoride; water; diisobutylaluminium hydride; toluene-4-sulfonic acid; triethylamine; N-ethyl-N,N-diisopropylamine; sodium bis(2-methoxyethoxy)aluminium dihydride; lithium diisopropyl amide; In tetrahydrofuran; diethyl ether; dichloromethane; dimethyl sulfoxide; 1,2-dichloro-ethane; benzene;
DOI:10.1016/j.tetlet.2012.01.058

Reference yield:

: 1365268-46-7
C₄₀H₅₄O₅Si

: 1365268-24-1
C₂₇H₄₂O₈

Guidance literature:: Multi-step reaction with 6 steps

1.1: hydrogenchloride; water / tetrahydrofuran / 20 °C

2.1: N-ethyl-N,N-diisopropylamine / 1,2-dichloro-ethane / 50 °C

3.1: lithium diisopropyl amide / tetrahydrofuran / -78 °C

3.2: -78 °C

4.1: N-ethyl-N,N-diisopropylamine / 1,2-dichloro-ethane / 50 °C

5.1: pyridine hydrofluoride / tetrahydrofuran / 0 °C

6.1: pig liver esterase; water / dimethyl sulfoxide / 17 h / 30 °C / pH 8 / aq. phosphate buffer; Enzymatic reaction

With hydrogenchloride; pig liver esterase; pyridine hydrofluoride; water; N-ethyl-N,N-diisopropylamine; lithium diisopropyl amide; In tetrahydrofuran; dimethyl sulfoxide; 1,2-dichloro-ethane;
DOI:10.1016/j.tetlet.2012.01.058