N-(adamantan-1-yl-2,2,8,8,9,9-d₆)-2-((2,4,6-trimethylphenyl)amino)acetamide

Base Information

Chemical Name:N-(adamantan-1-yl-2,2,8,8,9,9-d₆)-2-((2,4,6-trimethylphenyl)amino)acetamide
CAS No.:1600534-78-8
Molecular Formula:C₂₁H₃₀N₂O
Molecular Weight:332.434
Hs Code.:

N-(adamantan-1-yl-2,2,8,8,9,9-d<SUB>6</SUB>)-2-((2,4,6-trimethylphenyl)amino)acetamide

Synonyms:N-(adamantan-1-yl-2,2,8,8,9,9-d₆)-2-((2,4,6-trimethylphenyl)amino)acetamide

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Chemical Property of N-(adamantan-1-yl-2,2,8,8,9,9-d₆)-2-((2,4,6-trimethylphenyl)amino)acetamide

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Technology Process of N-(adamantan-1-yl-2,2,8,8,9,9-d₆)-2-((2,4,6-trimethylphenyl)amino)acetamide

There total 2 articles about N-(adamantan-1-yl-2,2,8,8,9,9-d₆)-2-((2,4,6-trimethylphenyl)amino)acetamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: 1600534-77-7
N-(adamantan-1-yl-2,2,8,8,9,9-d₆)-2-bromoacetamide

: 88-05-1
2,4,6-trimethylaniline

: 1600534-78-8
N-(adamantan-1-yl-2,2,8,8,9,9-d₆)-2-((2,4,6-trimethylphenyl)amino)acetamide

Guidance literature:: With potassium carbonate; In acetonitrile; at 130 ℃; for 0.5h; under 3000.3 Torr; Microwave irradiation;
DOI:10.1021/ja5021958

Reference yield:

: 1219805-53-4
C₁₀H₁₁⁽²⁾H₆N

: 1600534-78-8
N-(adamantan-1-yl-2,2,8,8,9,9-d₆)-2-((2,4,6-trimethylphenyl)amino)acetamide

Guidance literature:: Multi-step reaction with 2 steps

1: potassium carbonate / dichloromethane / 2.17 h / 0 - 20 °C / Cooling with ice

2: potassium carbonate / acetonitrile / 0.5 h / 130 °C / 3000.3 Torr / Microwave irradiation

With potassium carbonate; In dichloromethane; acetonitrile;
DOI:10.1021/ja5021958

Reference yield: 94.0%

: 1600534-78-8
N-(adamantan-1-yl-2,2,8,8,9,9-d₆)-2-((2,4,6-trimethylphenyl)amino)acetamide

: 1600534-79-9
C₂₁H₂₆⁽²⁾H₆N₂

Guidance literature:: With lithium aluminium tetrahydride; In tetrahydrofuran; at 130 ℃; for 1h; under 6000.6 Torr; Microwave irradiation;
DOI:10.1021/ja5021958