epi-5-[(2-amino-6-benzyloxypurin-9-yl)acetylamino]-5-deoxy-1,3,2',6'-tetraazido-6,3',4'-tri-O-benzylneamine

Base Information

Chemical Name:epi-5-[(2-amino-6-benzyloxypurin-9-yl)acetylamino]-5-deoxy-1,3,2',6'-tetraazido-6,3',4'-tri-O-benzylneamine
CAS No.:1432025-41-6
Molecular Formula:C₄₇H₄₈N₁₈O₇
Molecular Weight:977.015
Hs Code.:

Synonyms:epi-5-[(2-amino-6-benzyloxypurin-9-yl)acetylamino]-5-deoxy-1,3,2',6'-tetraazido-6,3',4'-tri-O-benzylneamine

Suppliers and Price of epi-5-[(2-amino-6-benzyloxypurin-9-yl)acetylamino]-5-deoxy-1,3,2',6'-tetraazido-6,3',4'-tri-O-benzylneamine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of epi-5-[(2-amino-6-benzyloxypurin-9-yl)acetylamino]-5-deoxy-1,3,2',6'-tetraazido-6,3',4'-tri-O-benzylneamine

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of epi-5-[(2-amino-6-benzyloxypurin-9-yl)acetylamino]-5-deoxy-1,3,2',6'-tetraazido-6,3',4'-tri-O-benzylneamine

There total 2 articles about epi-5-[(2-amino-6-benzyloxypurin-9-yl)acetylamino]-5-deoxy-1,3,2',6'-tetraazido-6,3',4'-tri-O-benzylneamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 49.0%

: 1432025-40-5
epi-5-amino-5-deoxy-1,3,2',6'-tetraazido-6,3',4'-tri-O-benzylneamine

: 149411-94-9
2-(2-amino-6-(benzyloxy)-9H-purin-9-yl)acetic acid

: 1432025-41-6
epi-5-[(2-amino-6-benzyloxypurin-9-yl)acetylamino]-5-deoxy-1,3,2',6'-tetraazido-6,3',4'-tri-O-benzylneamine

Guidance literature:: With O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; triethylamine; In N,N-dimethyl-formamide; at 20 ℃; for 36h; Inert atmosphere;
DOI:10.1016/j.cclet.2013.03.009

Reference yield:

: 5-O-triflyl-1,3,2',6'-tetraazido-6,3',4'-tri-O-benzylneamine

: 1432025-41-6
epi-5-[(2-amino-6-benzyloxypurin-9-yl)acetylamino]-5-deoxy-1,3,2',6'-tetraazido-6,3',4'-tri-O-benzylneamine

Guidance literature:: Multi-step reaction with 2 steps

1: ammonia / acetone / 2 h / Cooling with ice

2: triethylamine; O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate / N,N-dimethyl-formamide / 36 h / 20 °C / Inert atmosphere

With ammonia; O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; triethylamine; In N,N-dimethyl-formamide; acetone;
DOI:10.1016/j.cclet.2013.03.009