5-azideo-3,4-di-O-benzoyl-5-deoxy-1,2-O-isopropylidene-β-L-sorbopyranose

Base Information

Chemical Name:5-azideo-3,4-di-O-benzoyl-5-deoxy-1,2-O-isopropylidene-β-L-sorbopyranose
CAS No.:368452-21-5
Molecular Formula:C₂₃H₂₃N₃O₇
Molecular Weight:453.452
Hs Code.:

Synonyms:5-azideo-3,4-di-O-benzoyl-5-deoxy-1,2-O-isopropylidene-β-L-sorbopyranose

Suppliers and Price of 5-azideo-3,4-di-O-benzoyl-5-deoxy-1,2-O-isopropylidene-β-L-sorbopyranose

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 5-azideo-3,4-di-O-benzoyl-5-deoxy-1,2-O-isopropylidene-β-L-sorbopyranose

Chemical Property:

Purity/Quality:: 98% ^*data from raw suppliers

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Technology Process of 5-azideo-3,4-di-O-benzoyl-5-deoxy-1,2-O-isopropylidene-β-L-sorbopyranose

There total 7 articles about 5-azideo-3,4-di-O-benzoyl-5-deoxy-1,2-O-isopropylidene-β-L-sorbopyranose which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 368452-03-3
3,4-di-O-benzoyl-5-deoxy-5-iodo-1,2-O-isopropylidene-β-L-sorbopyranose

: 368452-21-5
5-azideo-3,4-di-O-benzoyl-5-deoxy-1,2-O-isopropylidene-β-L-sorbopyranose

Guidance literature:: With sodium azide; In dimethyl sulfoxide; at 100 ℃; for 3h;
DOI:10.1016/S0008-6215(01)00153-7

Reference yield:

: 99648-49-4
3-O-benzoyl-1,2-O-isopropylidene-β-D-fructopyranose

: 368452-21-5
5-azideo-3,4-di-O-benzoyl-5-deoxy-1,2-O-isopropylidene-β-L-sorbopyranose

Guidance literature:: Multi-step reaction with 3 steps

1: 90 percent / pyridine / 1.5 h / -65 °C

2: 98 percent / iodine; triphenylphosphine; imidazole / toluene / 70 °C

3: 91 percent / sodium azide; HMPT / 80 °C

With pyridine; 1H-imidazole; N,N,N,N,N,N-hexamethylphosphoric triamide; sodium azide; iodine; triphenylphosphine; In toluene;
DOI:10.1021/jo0499221

Reference yield:

: 99648-59-6
3,4-di-O-benzoyl-1,2-O-isopropylidene-β-D-fructopyranose

: 368452-21-5
5-azideo-3,4-di-O-benzoyl-5-deoxy-1,2-O-isopropylidene-β-L-sorbopyranose

Guidance literature:: Multi-step reaction with 2 steps

1: 98 percent / iodine; triphenylphosphine; imidazole / toluene / 70 °C

2: 91 percent / sodium azide; HMPT / 80 °C

With 1H-imidazole; N,N,N,N,N,N-hexamethylphosphoric triamide; sodium azide; iodine; triphenylphosphine; In toluene;
DOI:10.1021/jo0499221