1-(4-fluorophenyl)-3-butenyl N,N-bis(2-chloroethyl)phosphorodiamidate

Base Information

Chemical Name:1-(4-fluorophenyl)-3-butenyl N,N-bis(2-chloroethyl)phosphorodiamidate
CAS No.:136185-89-2
Molecular Formula:C₁₄H₂₀Cl₂FN₂O₂P
Molecular Weight:369.203
Hs Code.:

Synonyms:1-(4-fluorophenyl)-3-butenyl N,N-bis(2-chloroethyl)phosphorodiamidate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1-(4-fluorophenyl)-3-butenyl N,N-bis(2-chloroethyl)phosphorodiamidate

Chemical Property:

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Technology Process of 1-(4-fluorophenyl)-3-butenyl N,N-bis(2-chloroethyl)phosphorodiamidate

There total 3 articles about 1-(4-fluorophenyl)-3-butenyl N,N-bis(2-chloroethyl)phosphorodiamidate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₁₄H₁₈Cl₃FNO₂P

: 136185-89-2
1-(4-fluorophenyl)-3-butenyl N,N-bis(2-chloroethyl)phosphorodiamidate

Guidance literature:: With ammonia; In tetrahydrofuran; hexane; at 0 ℃; Yield given;
DOI:10.1021/jm00114a013

Reference yield:

: 459-57-4
4-fluorobenzaldehyde

: 136185-89-2
1-(4-fluorophenyl)-3-butenyl N,N-bis(2-chloroethyl)phosphorodiamidate

Guidance literature:: Multi-step reaction with 3 steps

1: 94 percent / SnF₂, DMI / dimethylformamide / Ambient temperature

2: 1.) (phenylazo)diphenylamine, n-BuLi, 2.) POCl₃ / 1.) THF, hexane, 0 deg C, 2.) THF, hexane, 0 deg C, 20 min

3: gaseous NH₃ / tetrahydrofuran; hexane / 0 °C

With stannous fluoride; n-butyllithium; desipramine; ammonia; 4-(Phenylazo)diphenylamine; trichlorophosphate; In tetrahydrofuran; hexane; N,N-dimethyl-formamide;
DOI:10.1021/jm00114a013

Reference yield:

: 86718-78-7,136185-86-9
1-(4-fluorophenyl)-3-buten-1-ol

: 136185-89-2
1-(4-fluorophenyl)-3-butenyl N,N-bis(2-chloroethyl)phosphorodiamidate

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) (phenylazo)diphenylamine, n-BuLi, 2.) POCl₃ / 1.) THF, hexane, 0 deg C, 2.) THF, hexane, 0 deg C, 20 min

2: gaseous NH₃ / tetrahydrofuran; hexane / 0 °C

With n-butyllithium; ammonia; 4-(Phenylazo)diphenylamine; trichlorophosphate; In tetrahydrofuran; hexane;
DOI:10.1021/jm00114a013