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ReCl4(((C6H5)2PCH)2)

Base Information
  • Chemical Name:ReCl4(((C6H5)2PCH)2)
  • CAS No.:110277-32-2
  • Molecular Formula:C26H22Cl4P2Re
  • Molecular Weight:724.427
  • Hs Code.:
ReCl<sub>4</sub>(((C<sub>6</sub>H<sub>5</sub>)2PCH)2)

Synonyms:ReCl4(((C6H5)2PCH)2)

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Chemical Property of ReCl4(((C6H5)2PCH)2)
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Technology Process of ReCl4(((C6H5)2PCH)2)

There total 2 articles about ReCl4(((C6H5)2PCH)2) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:
Guidance literature:
With CCl4; In tetrachloromethane; dichloromethane; β-Re2Cl4(dppee92, CH2Cl2 and CCl4 refluxed for 2 days; react. mixt. cooled to room temp., solvent evaporated, residue extracted into CH2Cl2, filtered, diethyl ether added to filtrate; elem. anal.;
DOI:10.1016/S0277-5387(00)80914-6
Guidance literature:
With CCl4; In tetrachloromethane; dichloromethane; α-Re2Cl4(dppee)2, CH2Cl2 and CCl4 refluxed for 2 days; react. mixt. cooled to room temp., solvent evaporated, residue extracted into CH2Cl2, filtered, diethyl ether added to filtrate; elem. anal.;
DOI:10.1016/S0277-5387(00)80914-6
upstream raw materials:

α-Re2Cl4(dppee)2

β-Re2Cl4(dppee)2

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