Phenyl-(2-phenyl-10b-p-tolyl-6b,10b-dihydro-1-oxa-benzo[2,3]pentaleno[1,6-ab]inden-10c-yl)-methanone

Base Information

Chemical Name:Phenyl-(2-phenyl-10b-p-tolyl-6b,10b-dihydro-1-oxa-benzo[2,3]pentaleno[1,6-ab]inden-10c-yl)-methanone
CAS No.:124562-66-9
Molecular Formula:C₃₇H₂₆O₂
Molecular Weight:502.612
Hs Code.:

Synonyms:Phenyl-(2-phenyl-10b-p-tolyl-6b,10b-dihydro-1-oxa-benzo[2,3]pentaleno[1,6-ab]inden-10c-yl)-methanone

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Chemical Property of Phenyl-(2-phenyl-10b-p-tolyl-6b,10b-dihydro-1-oxa-benzo[2,3]pentaleno[1,6-ab]inden-10c-yl)-methanone

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Technology Process of Phenyl-(2-phenyl-10b-p-tolyl-6b,10b-dihydro-1-oxa-benzo[2,3]pentaleno[1,6-ab]inden-10c-yl)-methanone

There total 3 articles about Phenyl-(2-phenyl-10b-p-tolyl-6b,10b-dihydro-1-oxa-benzo[2,3]pentaleno[1,6-ab]inden-10c-yl)-methanone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 124562-60-3
C₃₇H₂₆O₂

: 124562-66-9
Phenyl-(2-phenyl-10b-p-tolyl-6b,10b-dihydro-1-oxa-benzo[2,3]pentaleno[1,6-ab]inden-10c-yl)-methanone

Guidance literature:: In benzene; for 2h; Irradiation;
DOI:10.1021/jo00291a039

Reference yield:

: 1087-09-8
1,4-diphenyl-but-2-yne-1,4-dione

: 124562-66-9
Phenyl-(2-phenyl-10b-p-tolyl-6b,10b-dihydro-1-oxa-benzo[2,3]pentaleno[1,6-ab]inden-10c-yl)-methanone

Guidance literature:: Multi-step reaction with 2 steps

1: 83 percent / AlCl₃ / CHCl₃ / 1 h / 0 - 5 °C

2: 15 percent Spectr_. / benzene-d6 / 1 h / 15 °C / Irradiation

With aluminium trichloride; In chloroform; benzene-d6;
DOI:10.1021/jo00291a039

Reference yield:

: 23674-14-8
9-(4-methylphenyl)anthracene

: 124562-66-9
Phenyl-(2-phenyl-10b-p-tolyl-6b,10b-dihydro-1-oxa-benzo[2,3]pentaleno[1,6-ab]inden-10c-yl)-methanone

Guidance literature:: Multi-step reaction with 2 steps

1: 83 percent / AlCl₃ / CHCl₃ / 1 h / 0 - 5 °C

2: 15 percent Spectr_. / benzene-d6 / 1 h / 15 °C / Irradiation

With aluminium trichloride; In chloroform; benzene-d6;
DOI:10.1021/jo00291a039