[palladium(II)chloride(PPh3)(η5-C5H5)iron(II)(η5-C5H3(NC5H3(NHC6H5)))]

Base Information

Chemical Name:[palladium(II)chloride(PPh3)(η5-C5H5)iron(II)(η5-C5H3(NC5H3(NHC6H5)))]
CAS No.:1350659-46-9
Molecular Formula:C₃₉H₃₂ClFeN₂PPd
Molecular Weight:757.39
Hs Code.:

Synonyms:[palladium(II)chloride(PPh3)(η5-C5H5)iron(II)(η5-C5H3(NC5H3(NHC6H5)))]

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Chemical Property of [palladium(II)chloride(PPh3)(η5-C5H5)iron(II)(η5-C5H3(NC5H3(NHC6H5)))]

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Technology Process of [palladium(II)chloride(PPh3)(η5-C5H5)iron(II)(η5-C5H3(NC5H3(NHC6H5)))]

There total 1 articles about [palladium(II)chloride(PPh3)(η5-C5H5)iron(II)(η5-C5H3(NC5H3(NHC6H5)))] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 1350659-26-5
[palladium(II)chloride(PPh3)(η5-C5H5)iron(II)(η5-C5H3(NC5H3Br))]

: 62-53-3
aniline

: 1350659-46-9
[palladium(II)chloride(PPh3)(η5-C5H5)iron(II)(η5-C5H3(NC5H3(NHC6H5)))]

Guidance literature:: With KOtBu; [(η5-C5H5)iron(II)(η5-C5H3N2C4H(CH3)2PdClP(C6H11)2(C12H8(N(CH3)2)))]; In 1,4-dioxane; Schlenk technique, under N2: react. of Fe complex (0.5 mmol) and C6H5NH2(0.75 mmol) in presence of KOtBu (1 mmol) and Pd catalyst (0.001 equiv. ) at 110°C for 24 h, quenched in H2O; organic layer sepd., aq. layer extracted with CH2Cl2, combined organic layer washed with H2O, dried with MgSO4, filtered, solvent evapd., chromd. (silica gel);
DOI:10.1002/ejic.201100617