10-[4-[(Diphenylphosphinyl)amino]benzoyl]-10,11-dihydro-5H-pyrrolo-[2,1-c][1,4]benzodiazepine

Base Information

Chemical Name:10-[4-[(Diphenylphosphinyl)amino]benzoyl]-10,11-dihydro-5H-pyrrolo-[2,1-c][1,4]benzodiazepine
CAS No.:168079-42-3
Molecular Formula:C₃₁H₂₆N₃O₂P
Molecular Weight:503.54
Hs Code.:

Synonyms:10-[4-[(Diphenylphosphinyl)amino]benzoyl]-10,11-dihydro-5H-pyrrolo-[2,1-c][1,4]benzodiazepine

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Chemical Property of 10-[4-[(Diphenylphosphinyl)amino]benzoyl]-10,11-dihydro-5H-pyrrolo-[2,1-c][1,4]benzodiazepine

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Technology Process of 10-[4-[(Diphenylphosphinyl)amino]benzoyl]-10,11-dihydro-5H-pyrrolo-[2,1-c][1,4]benzodiazepine

There total 7 articles about 10-[4-[(Diphenylphosphinyl)amino]benzoyl]-10,11-dihydro-5H-pyrrolo-[2,1-c][1,4]benzodiazepine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 168078-59-9
10,11-dihydro-10-(4-aminobenzoyl)-5H-pyrrolo[2,1-c][1,4]benzodiazepine

: 1499-21-4
Diphenylphosphinic chloride

: 168079-42-3
10-[4-[(Diphenylphosphinyl)amino]benzoyl]-10,11-dihydro-5H-pyrrolo-[2,1-c][1,4]benzodiazepine

Guidance literature:: With sodium hydroxide; In dichloromethane;

Reference yield:

: 168078-58-8
10,11-dihydro-10(4-nitrobenzoyl)-5H-pyrrolo[2,1-c][1,4]benzodiazepine

: 168079-42-3
10-[4-[(Diphenylphosphinyl)amino]benzoyl]-10,11-dihydro-5H-pyrrolo-[2,1-c][1,4]benzodiazepine

Guidance literature:: Multi-step reaction with 2 steps

1: hydrazine / palladium-carbon / ethanol

2: sodium hydroxide / dichloromethane

With sodium hydroxide; hydrazine; palladium-carbon; In ethanol; dichloromethane;

Reference yield:

: 1003-29-8,254729-95-8
2-pyrrole aldehyde

: 168079-42-3
10-[4-[(Diphenylphosphinyl)amino]benzoyl]-10,11-dihydro-5H-pyrrolo-[2,1-c][1,4]benzodiazepine

Guidance literature:: Multi-step reaction with 5 steps

1: sodium hydride / 2-pyrrole aldehyde; N,N-dimethyl-formamide; mineral oil

2: hydrogen / palladium-carbon / ethanol; ethyl acetate

3: triethylamine / dichloromethane

4: hydrazine / palladium-carbon / ethanol

5: triethylamine / dichloromethane

With sodium hydride; hydrogen; triethylamine; hydrazine; palladium-carbon; In 2-pyrrole aldehyde; ethanol; dichloromethane; ethyl acetate; N,N-dimethyl-formamide; mineral oil;