Technology Process of C41H39ClF2O6
There total 3 articles about C41H39ClF2O6 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
n-butyllithium;
In
tetrahydrofuran; diethyl ether; hexane; pentane;
at -90 ℃;
for 1.5h;
Inert atmosphere;
- Guidance literature:
-
Multi-step reaction with 3 steps
1: diethylamino-sulfur trifluoride / methanol / dichloromethane / 20 °C / Inert atmosphere
2: bromine; potassium carbonate / tetrachloromethane / 5 h / Inert atmosphere; UV-irradiation; Reflux
3: n-butyllithium / tetrahydrofuran; diethyl ether; hexane; pentane / 1.5 h / -90 °C / Inert atmosphere
With
n-butyllithium; diethylamino-sulfur trifluoride; bromine; potassium carbonate;
methanol;
In
tetrahydrofuran; tetrachloromethane; diethyl ether; hexane; dichloromethane; pentane;
3: Barbier Reaction;
- Guidance literature:
-
Multi-step reaction with 2 steps
1: bromine; potassium carbonate / tetrachloromethane / 5 h / Inert atmosphere; UV-irradiation; Reflux
2: n-butyllithium / tetrahydrofuran; diethyl ether; hexane; pentane / 1.5 h / -90 °C / Inert atmosphere
With
n-butyllithium; bromine; potassium carbonate;
In
tetrahydrofuran; tetrachloromethane; diethyl ether; hexane; pentane;
2: Barbier Reaction;