1,2-bis(3-hydroxy-1-phenyl-1,2,3,4-tetrahydroquinoline-6-ylmethylene)azine

Base Information

Chemical Name:1,2-bis(3-hydroxy-1-phenyl-1,2,3,4-tetrahydroquinoline-6-ylmethylene)azine
CAS No.:1330779-11-7
Molecular Formula:C₃₂H₃₀N₄O₂
Molecular Weight:502.616
Hs Code.:

Synonyms:1,2-bis(3-hydroxy-1-phenyl-1,2,3,4-tetrahydroquinoline-6-ylmethylene)azine

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Chemical Property of 1,2-bis(3-hydroxy-1-phenyl-1,2,3,4-tetrahydroquinoline-6-ylmethylene)azine

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Technology Process of 1,2-bis(3-hydroxy-1-phenyl-1,2,3,4-tetrahydroquinoline-6-ylmethylene)azine

There total 3 articles about 1,2-bis(3-hydroxy-1-phenyl-1,2,3,4-tetrahydroquinoline-6-ylmethylene)azine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: rac-3-hydroxy-1-phenyl-1,2,3,4-tetrahydroquinoline-6-carbaldehyde

: 1330779-11-7
1,2-bis(3-hydroxy-1-phenyl-1,2,3,4-tetrahydroquinoline-6-ylmethylene)azine

Guidance literature:: With hydrazine hydrate; In tetrahydrofuran; for 1h; Reflux;
DOI:10.1016/j.reactfunctpolym.2011.07.005

Reference yield:

: 934420-64-1
3-acetyl-1-phenyl-1,2,3,4-tetrahydroquinoline-6-carbaldehyde

: 1330779-11-7
1,2-bis(3-hydroxy-1-phenyl-1,2,3,4-tetrahydroquinoline-6-ylmethylene)azine

Guidance literature:: Multi-step reaction with 2 steps

1: potassium hydroxide

2: hydrazine hydrate / tetrahydrofuran / 1 h / Reflux

With hydrazine hydrate; potassium hydroxide; In tetrahydrofuran;
DOI:10.1016/j.reactfunctpolym.2011.07.005

Reference yield:

: 3297-78-7
acetic acid 1-phenyl-1,2,3,4-tetrahydro-quinolin-3-yl ester

: 1330779-11-7
1,2-bis(3-hydroxy-1-phenyl-1,2,3,4-tetrahydroquinoline-6-ylmethylene)azine

Guidance literature:: Multi-step reaction with 3 steps

1: trichlorophosphate

2: potassium hydroxide

3: hydrazine hydrate / tetrahydrofuran / 1 h / Reflux

With hydrazine hydrate; potassium hydroxide; trichlorophosphate; In tetrahydrofuran;
DOI:10.1016/j.reactfunctpolym.2011.07.005