(S)-1-O-(4,4'-dimethoxytrityl)-3-O-[4-(pyren-1-ylethynyl)phenylmethyl]glycerol

Base Information

Chemical Name:(S)-1-O-(4,4'-dimethoxytrityl)-3-O-[4-(pyren-1-ylethynyl)phenylmethyl]glycerol
CAS No.:914675-37-9
Molecular Formula:C₄₉H₄₀O₅
Molecular Weight:708.854
Hs Code.:

Synonyms:(S)-1-O-(4,4'-dimethoxytrityl)-3-O-[4-(pyren-1-ylethynyl)phenylmethyl]glycerol

Suppliers and Price of (S)-1-O-(4,4'-dimethoxytrityl)-3-O-[4-(pyren-1-ylethynyl)phenylmethyl]glycerol

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (S)-1-O-(4,4'-dimethoxytrityl)-3-O-[4-(pyren-1-ylethynyl)phenylmethyl]glycerol

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Technology Process of (S)-1-O-(4,4'-dimethoxytrityl)-3-O-[4-(pyren-1-ylethynyl)phenylmethyl]glycerol

There total 3 articles about (S)-1-O-(4,4'-dimethoxytrityl)-3-O-[4-(pyren-1-ylethynyl)phenylmethyl]glycerol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 34993-56-1
1-ethynylpyrene

: 914675-37-9
(S)-1-O-(4,4'-dimethoxytrityl)-3-O-[4-(pyren-1-ylethynyl)phenylmethyl]glycerol

Guidance literature:: Multi-step reaction with 2 steps

1: 3.1 g / Et₃N; CuI; Pd(PPh₃)4 / dimethylformamide / 20 °C

2: 1.75 g / pyridine / 40 h / 20 °C

With copper(l) iodide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; triethylamine; In pyridine; N,N-dimethyl-formamide; 1: Sonogashira coupling;
DOI:10.1002/ejoc.200600168

Reference yield:

: 869670-01-9
(R)-3-(4-iodobenzyloxy)propane-1,2-diol

: 914675-37-9
(S)-1-O-(4,4'-dimethoxytrityl)-3-O-[4-(pyren-1-ylethynyl)phenylmethyl]glycerol

Guidance literature:: Multi-step reaction with 2 steps

1: 3.1 g / Et₃N; CuI; Pd(PPh₃)4 / dimethylformamide / 20 °C

2: 1.75 g / pyridine / 40 h / 20 °C

With copper(l) iodide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; triethylamine; In pyridine; N,N-dimethyl-formamide; 1: Sonogashira coupling;
DOI:10.1002/ejoc.200600168