thiocarbonic acid O-[1-(2-bromo-phenyl)-2,2,2-trifluoro-ethyl] ester O-phenyl ester

Base Information

Chemical Name:thiocarbonic acid O-[1-(2-bromo-phenyl)-2,2,2-trifluoro-ethyl] ester O-phenyl ester
CAS No.:1221349-89-8
Molecular Formula:C₁₅H₁₀BrF₃O₂S
Molecular Weight:391.208
Hs Code.:

Synonyms:thiocarbonic acid O-[1-(2-bromo-phenyl)-2,2,2-trifluoro-ethyl] ester O-phenyl ester

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of thiocarbonic acid O-[1-(2-bromo-phenyl)-2,2,2-trifluoro-ethyl] ester O-phenyl ester

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Technology Process of thiocarbonic acid O-[1-(2-bromo-phenyl)-2,2,2-trifluoro-ethyl] ester O-phenyl ester

There total 1 articles about thiocarbonic acid O-[1-(2-bromo-phenyl)-2,2,2-trifluoro-ethyl] ester O-phenyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1005-56-7
phenylcarbonochloridothioate

: 394203-55-5
1-(2-bromophenyl)-2,2,2-trifluoroethanol

: 1221349-89-8
thiocarbonic acid O-[1-(2-bromo-phenyl)-2,2,2-trifluoro-ethyl] ester O-phenyl ester

Guidance literature:: With triethylamine; In dichloromethane; at 20 ℃; Cooling with water bath;

Reference yield: 34.0%

: 1221349-89-8
thiocarbonic acid O-[1-(2-bromo-phenyl)-2,2,2-trifluoro-ethyl] ester O-phenyl ester

: 1027513-81-0
1-bromo-2-(2,2,2-trifluoroethyl)benzene

Guidance literature:: thiocarbonic acid O-[1-(2-bromo-phenyl)-2,2,2-trifluoro-ethyl] ester O-phenyl ester; With 2,2'-azobis(isobutyronitrile); bis(tri-n-butyltin)oxide; In toluene; butan-1-ol; at 80 ℃; for 28h; Polymethylhydrosiloxane (PMHS)

With sodium hydroxide; In tetrahydrofuran; water; toluene; butan-1-ol; at 20 ℃; for 12h;