methyl-2,2-dimethylcyclopropyl ketone cyclic (1S,2S)-1,2-bis<(benzyloxy)methyl>ethylene acetal

Base Information

Chemical Name:methyl-2,2-dimethylcyclopropyl ketone cyclic (1S,2S)-1,2-bis<(benzyloxy)methyl>ethylene acetal
CAS No.:110678-03-0
Molecular Formula:C₂₅H₃₂O₄
Molecular Weight:396.527
Hs Code.:

Synonyms:methyl-2,2-dimethylcyclopropyl ketone cyclic (1S,2S)-1,2-bis<(benzyloxy)methyl>ethylene acetal

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Chemical Property of methyl-2,2-dimethylcyclopropyl ketone cyclic (1S,2S)-1,2-bis<(benzyloxy)methyl>ethylene acetal

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Technology Process of methyl-2,2-dimethylcyclopropyl ketone cyclic (1S,2S)-1,2-bis<(benzyloxy)methyl>ethylene acetal

There total 3 articles about methyl-2,2-dimethylcyclopropyl ketone cyclic (1S,2S)-1,2-bis<(benzyloxy)methyl>ethylene acetal which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 17401-06-8
(2S,3S)-1,4-bis(benzyloxy)-2,3-butanediol

: 110678-03-0
methyl-2,2-dimethylcyclopropyl ketone cyclic (1S,2S)-1,2-bis<(benzyloxy)methyl>ethylene acetal

Guidance literature:: Multi-step reaction with 2 steps

1: 86 percent / pyridinium p-toluenesulfonate / benzene / Heating

2: zinc-copper couple / iodine / diethyl ether / 0.5 h / Heating

With zinc copper; iodine; pyridinium p-toluenesulfonate; In diethyl ether; benzene;
DOI:10.1016/S0040-4020(01)90002-X

Reference yield:

: 141-79-7
4-methyl-pent-3-en-2-one

: 110678-03-0
methyl-2,2-dimethylcyclopropyl ketone cyclic (1S,2S)-1,2-bis<(benzyloxy)methyl>ethylene acetal

Guidance literature:: Multi-step reaction with 2 steps

1: 86 percent / pyridinium p-toluenesulfonate / benzene / Heating

2: zinc-copper couple / iodine / diethyl ether / 0.5 h / Heating

With zinc copper; iodine; pyridinium p-toluenesulfonate; In diethyl ether; benzene;
DOI:10.1016/S0040-4020(01)90002-X

Reference yield:

: 75-11-6
diiodomethane

: 110677-98-0
4-methyl-3-penten-2-one cyclic (1S,2S)-1,2-bis<(benzyloxy)methyl>ethylene acetal

: 110678-02-9
methyl-2,2-dimethylcyclopropyl ketone cyclic (1S,2S)-1,2-bis<(benzyloxy)methyl>ethylene acetal

: 110678-03-0
methyl-2,2-dimethylcyclopropyl ketone cyclic (1S,2S)-1,2-bis<(benzyloxy)methyl>ethylene acetal

Guidance literature:: With zinc copper; iodine; In diethyl ether; for 0.5h; Yield given. Yields of byproduct given. Title compound not separated from byproducts; Heating;
DOI:10.1016/S0040-4020(01)90002-X