[2,4,6-tris[bis(trimethylsilyl)methyl]phenyl][bis(trimethylsilyl)methyl]germanethione

Base Information

• Chemical Name: [2,4,6-tris[bis(trimethylsilyl)methyl]phenyl][bis(trimethylsilyl)methyl]germanethione
• CAS No.: 247245-92-7
• Molecular Formula: C₃₄H₇₈GeSSi₈
• Molecular Weight: 816.333

Synonyms:[2,4,6-tris[bis(trimethylsilyl)methyl]phenyl][bis(trimethylsilyl)methyl]germanethione

Chemical Property of [2,4,6-tris[bis(trimethylsilyl)methyl]phenyl][bis(trimethylsilyl)methyl]germanethione

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of [2,4,6-tris[bis(trimethylsilyl)methyl]phenyl][bis(trimethylsilyl)methyl]germanethione

There total 15 articles about [2,4,6-tris[bis(trimethylsilyl)methyl]phenyl][bis(trimethylsilyl)methyl]germanethione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 62.0%

5-[2,4,6-tris[bis(trimethylsilyl)methyl]phenyl]-5-[bis(trimethylsilyl)methyl]-1,2,3,4,5-tertathiagermolane + triphenylphosphine (603-35-0) → [2,4,6-tris[bis(trimethylsilyl)methyl]phenyl][bis(trimethylsilyl)methyl]germanethione (247245-92-7) + 3,6-bis[bis(trimethylsilyl)methyl]-3,6-bis[2,4,6-tris[bis(trimethylsilyl)methyl]phenyl]-1,2,4,5-tetrathia-3,6-digermacyclohexane

Guidance literature:

In hexane; byproducts: Ph3PS; refluxing (3 h); filtration, concentration (Ar);

DOI:10.1021/ja991147x

Reference yield: 62.0%

GeS4(CH(Si(CH3)3)2)(C6H2(CH(Si(CH3)3)2)3) (247245-77-8) → [2,4,6-tris[bis(trimethylsilyl)methyl]phenyl][bis(trimethylsilyl)methyl]germanethione (247245-92-7) + [GeS2(CH(Si(CH3)3)2)(C6H2(CH(Si(CH3)3)2)3)]2 (247245-79-0)

Guidance literature:

With triphenylphosphine; In hexane; byproducts: Ph3PS; 3 equiv. PPh3, heating;

DOI:10.1246/bcsj.72.1665

Reference yield:

sulfur (10544-50-0) + 2,3-diphenyl-1-[2,4,6-tris[bis(trimethylsilyl)methyl]phenyl]-1-[bis(trimethylsilyl)methyl]germirene → [2,4,6-tris[bis(trimethylsilyl)methyl]phenyl][bis(trimethylsilyl)methyl]germanethione (247245-92-7)

Guidance literature:

In benzene-d6; freezing, evacuation, sealing, heating (90°C, 10 h);

DOI:10.1021/ja991147x

upstream raw materials:

GeS₄(CH(Si(CH₃)3)2)(C₆H₂(CH(Si(CH₃)3)2)3)

triphenylphosphine

sulfur

[2,4,6-tris[bis(trimethylsilyl)methyl]phenyl][bis(trimethylsilyl)methyl]germylene

Downstream raw materials:

diphenyl acetylene

Post a RFQ

Cas No.:

Product Name:

Quantity:

Please select Metric Ton KG G Pound L ML

Email:

Company name:

Valid Period:

Detailed Requirements:

• Sample
• MOQ
• GMP
• FDA
• Price
  FOB CIF CFR EXW
• Urgent purchase

Enter 15 to 2000 letters.Word count: 0 letters

Attach files(File Format: Jpeg, Jpg, Gif, Png, PDF, PPT, Zip, Rar,Word or Excel Maximum File Size: 3MB)

Remove

Submit

1

What can I do for you?
Get Best Price

Get Best Price for 247245-92-7 [2,4,6-tris[bis(trimethylsilyl)methyl]phenyl][bis(trimethylsilyl)methyl]germanethione

Send

Send

Metric Ton KG G Pound L ML

Send

Send