3-N-benzyloxymethyl-3'-O-(tert-butyldiphenylsilyl)-5'-deoxy-5'-hydroxyamino-2'-O-methanesulfonyluridine

Base Information

Chemical Name:3-N-benzyloxymethyl-3'-O-(tert-butyldiphenylsilyl)-5'-deoxy-5'-hydroxyamino-2'-O-methanesulfonyluridine
CAS No.:1080623-51-3
Molecular Formula:C₃₄H₄₁N₃O₉SSi
Molecular Weight:695.866
Hs Code.:

Synonyms:3-N-benzyloxymethyl-3'-O-(tert-butyldiphenylsilyl)-5'-deoxy-5'-hydroxyamino-2'-O-methanesulfonyluridine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 3-N-benzyloxymethyl-3'-O-(tert-butyldiphenylsilyl)-5'-deoxy-5'-hydroxyamino-2'-O-methanesulfonyluridine

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Technology Process of 3-N-benzyloxymethyl-3'-O-(tert-butyldiphenylsilyl)-5'-deoxy-5'-hydroxyamino-2'-O-methanesulfonyluridine

There total 1 articles about 3-N-benzyloxymethyl-3'-O-(tert-butyldiphenylsilyl)-5'-deoxy-5'-hydroxyamino-2'-O-methanesulfonyluridine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₄₄H₅₇N₃O₁₃SSi

: 1080623-51-3
3-N-benzyloxymethyl-3'-O-(tert-butyldiphenylsilyl)-5'-deoxy-5'-hydroxyamino-2'-O-methanesulfonyluridine

Guidance literature:: C₄₄H₅₇N₃O₁₃SSi; With trifluoroacetic acid; In dichloromethane; at 20 ℃; for 4h; Inert atmosphere;

With sodium hydrogencarbonate; In dichloromethane; water;
DOI:10.1016/j.tet.2008.12.073

Reference yield: 53.0%

: 1080623-51-3
3-N-benzyloxymethyl-3'-O-(tert-butyldiphenylsilyl)-5'-deoxy-5'-hydroxyamino-2'-O-methanesulfonyluridine

: 1080623-52-4,1138083-38-1
(2S,8R,10R,12S)-5-(benzyloxymethyl)-11-(tert-butyldiphenylsilyloxy)-9,13-dioxa-1,5,7-triazatetracyclo[8.3.1.0(2,7).0(8,12)]tetradecane-4,6-dione

Guidance literature:: With potassium hexamethylsilazane; In tetrahydrofuran; toluene; at 0 ℃; for 0.5h; Inert atmosphere;
DOI:10.1016/j.tet.2008.12.073