(R)-di-tert-butyl 2,2'-(1-hydroxy-3-phenylpropan-2-ylazanediyl)diacetate

Base Information

Chemical Name:(R)-di-tert-butyl 2,2'-(1-hydroxy-3-phenylpropan-2-ylazanediyl)diacetate
CAS No.:1201813-99-1
Molecular Formula:C₂₁H₃₃NO₅
Molecular Weight:379.497
Hs Code.:

Synonyms:(R)-di-tert-butyl 2,2'-(1-hydroxy-3-phenylpropan-2-ylazanediyl)diacetate

Suppliers and Price of (R)-di-tert-butyl 2,2'-(1-hydroxy-3-phenylpropan-2-ylazanediyl)diacetate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (R)-di-tert-butyl 2,2'-(1-hydroxy-3-phenylpropan-2-ylazanediyl)diacetate

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Technology Process of (R)-di-tert-butyl 2,2'-(1-hydroxy-3-phenylpropan-2-ylazanediyl)diacetate

There total 1 articles about (R)-di-tert-butyl 2,2'-(1-hydroxy-3-phenylpropan-2-ylazanediyl)diacetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

: 5292-43-3
bromoacetic acid tert-butyl ester

: 5267-64-1
(R)-2-amino-3-phenylpropanol

: 1201813-99-1
(R)-di-tert-butyl 2,2'-(1-hydroxy-3-phenylpropan-2-ylazanediyl)diacetate

Guidance literature:: With potassium carbonate; In acetonitrile; at 0 - 20 ℃;
DOI:10.1021/jo901893n

Reference yield: 97.0%

: 1201813-99-1
(R)-di-tert-butyl 2,2'-(1-hydroxy-3-phenylpropan-2-ylazanediyl)diacetate

: 1201814-18-7
(R)-di-tert-butyl 2,2'-(2-iodo-3-phenylpropylazanediyl)diacetate

Guidance literature:: With 1H-imidazole; iodine; triphenylphosphine; In dichloromethane; at 0 - 20 ℃; optical yield given as %ee;
DOI:10.1021/jo901893n

Reference yield: 71.0%

: 1201813-99-1
(R)-di-tert-butyl 2,2'-(1-hydroxy-3-phenylpropan-2-ylazanediyl)diacetate

: tert-butyl 2-{[(2S)-2-bromo-3-phenylpropyl][2-(tert-butoxy)-2-oxoethyl]amino}acetate

Guidance literature:: With N-Bromosuccinimide; triphenylphosphine; In chloroform; at 0 - 20 ℃; for 5h; stereospecific reaction;
DOI:10.1039/c5ra11306g