C₂₆H₂₅N₅O

Base Information

Chemical Name:C₂₆H₂₅N₅O
CAS No.:1424869-59-9
Molecular Formula:C₂₆H₂₅N₅O
Molecular Weight:423.517
Hs Code.:

C<sub>26</sub>H<sub>25</sub>N<sub>5</sub>O

Synonyms:C₂₆H₂₅N₅O

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Chemical Property of C₂₆H₂₅N₅O

Chemical Property:

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Technology Process of C₂₆H₂₅N₅O

There total 6 articles about C₂₆H₂₅N₅O which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 1424869-76-0
5-[3-methoxy-5-(1-methyl-prop-2-ynyl)phenyl]isoquinoline

: 514854-13-8
2,4-diamino-6-ethyl-5-iodopyrimidine

: 1424869-59-9
C₂₆H₂₅N₅O

Guidance literature:: With bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; triethylamine; In N,N-dimethyl-formamide; at 65 ℃; for 12h; Inert atmosphere;
DOI:10.1016/j.bmcl.2013.01.008

Reference yield:

: 1073642-71-3
1-(3-bromo-5-methoxyphenyl)ethanone

: 1424869-59-9
C₂₆H₂₅N₅O

Guidance literature:: Multi-step reaction with 5 steps

1.1: caesium carbonate; bis-triphenylphosphine-palladium(II) chloride / 1,4-dioxane / 12 h / 80 °C / Inert atmosphere

2.1: sodium t-butanolate / tetrahydrofuran / 0.5 h / 0 °C / Inert atmosphere

2.2: 0.33 h / Inert atmosphere

3.1: mercury(II) diacetate / tetrahydrofuran; water / 2 h / 20 °C / Inert atmosphere

3.2: 0.25 h / Inert atmosphere

4.1: potassium carbonate / methanol / 1.5 h / 20 °C

5.1: bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; triethylamine / N,N-dimethyl-formamide / 12 h / 65 °C / Inert atmosphere

With bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; mercury(II) diacetate; potassium carbonate; caesium carbonate; triethylamine; sodium t-butanolate; In tetrahydrofuran; 1,4-dioxane; methanol; water; N,N-dimethyl-formamide; 1.1: |Suzuki Coupling / 2.2: |Wittig Olefination / 3.1: |Wittig Olefination / 4.1: |Wittig Olefination / 5.1: |Sonogashira Cross-Coupling;
DOI:10.1016/j.bmcl.2013.01.008

Reference yield:

: 371766-08-4
isoquinoline 5-boronic acid

: 1424869-59-9
C₂₆H₂₅N₅O

Guidance literature:: Multi-step reaction with 5 steps

1.1: caesium carbonate; bis-triphenylphosphine-palladium(II) chloride / 1,4-dioxane / 12 h / 80 °C / Inert atmosphere

2.1: sodium t-butanolate / tetrahydrofuran / 0.5 h / 0 °C / Inert atmosphere

2.2: 0.33 h / Inert atmosphere

3.1: mercury(II) diacetate / tetrahydrofuran; water / 2 h / 20 °C / Inert atmosphere

3.2: 0.25 h / Inert atmosphere

4.1: potassium carbonate / methanol / 1.5 h / 20 °C

5.1: bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; triethylamine / N,N-dimethyl-formamide / 12 h / 65 °C / Inert atmosphere

With bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; mercury(II) diacetate; potassium carbonate; caesium carbonate; triethylamine; sodium t-butanolate; In tetrahydrofuran; 1,4-dioxane; methanol; water; N,N-dimethyl-formamide; 1.1: |Suzuki Coupling / 2.2: |Wittig Olefination / 3.1: |Wittig Olefination / 4.1: |Wittig Olefination / 5.1: |Sonogashira Cross-Coupling;
DOI:10.1016/j.bmcl.2013.01.008