HCCC₆H₄((C₂)Pt(P(C₄H₉)3)2(C₂C₆H₄))4CCH

Base Information

• Chemical Name: HCCC₆H₄((C₂)Pt(P(C₄H₉)3)2(C₂C₆H₄))4CCH
• CAS No.: 1173397-67-5
• Molecular Formula: C₁₄₆H₂₃₈P₈Pt₄
• Molecular Weight: 3021.61

Synonyms:HCCC₆H₄((C₂)Pt(P(C₄H₉)3)2(C₂C₆H₄))4CCH

Chemical Property of HCCC₆H₄((C₂)Pt(P(C₄H₉)3)2(C₂C₆H₄))4CCH

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Technology Process of HCCC₆H₄((C₂)Pt(P(C₄H₉)3)2(C₂C₆H₄))4CCH

There total 1 articles about HCCC₆H₄((C₂)Pt(P(C₄H₉)3)2(C₂C₆H₄))4CCH which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

((CH3)2CH)3SiCCC6H4((C2)Pt(P(C4H9)3)2(C2C6H4))4CCSi(CH(CH3)2)3 → HCCC6H4((C2)Pt(P(C4H9)3)2(C2C6H4))4CCH (1173397-67-5)

Guidance literature:

With tetrabutyl ammonium fluoride; In tetrahydrofuran; room temp., 1 h;

DOI:10.1021/om900195p

Reference yield: 90.0%

PtCl(P(C4H9)3)2(C2C6H4C2)Pt(P(C4H9)3)2(C2C6H4C2Si(CH(CH3)2)3) (1173397-60-8) + HCCC6H4((C2)Pt(P(C4H9)3)2(C2C6H4))4CCH (1173397-67-5) → 2((CH3)2CH)3SiCCC6H4C2(1-)*8Pt(2+)*16P(C4H9)3*7C2C6H4C2(2-)=(C3H7)3SiCCC6H4((C2)Pt(P(C4H9)3)2(C2C6H4))8CCSi(C3H7)3

Guidance literature:

With diethylamine; copper(l) iodide; In tetrahydrofuran; diethylamine; two Pt complexes reacted in Et2NH-THF in presence of CuI at room temp. for 4 h;

DOI:10.1021/om900195p

Reference yield: 50.1%

[PtCl(PBu3)2(naphthalene diimide)] (1173397-64-2) + HCCC6H4((C2)Pt(P(C4H9)3)2(C2C6H4))4CCH (1173397-67-5) → C8H17NC14H4O4NC6H4(CCPt(PBu3)2CC(1,4-phenylene))6C14H4O4NC8H17

Guidance literature:

With diethylamine; copper(l) iodide; In tetrahydrofuran; under Ar; soln. of two Pt complexes and Et2NH in THF degassed with Ar for 5 min; CuI added; stirred at room temp. for 3 h; quenched with deionized H2O; diluted with CH2Cl2; washed with brine; org. layer dried (Na2SO4); solvent removed; purified by flash chromy. (silica gel, CHCl3-hexane 2:1); red band collected; solvent removed; elem. anal.;

DOI:10.1021/om900195p

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