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dodecyl 4'-hydroxybiphenyl-4-carboxylate

Base Information Edit
  • Chemical Name:dodecyl 4'-hydroxybiphenyl-4-carboxylate
  • CAS No.:132328-90-6
  • Molecular Formula:C25H34O3
  • Molecular Weight:382.543
  • Hs Code.:
  • Mol file:132328-90-6.mol
dodecyl 4'-hydroxybiphenyl-4-carboxylate

Synonyms:dodecyl 4'-hydroxybiphenyl-4-carboxylate

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Chemical Property of dodecyl 4'-hydroxybiphenyl-4-carboxylate Edit
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Technology Process of dodecyl 4'-hydroxybiphenyl-4-carboxylate

There total 1 articles about dodecyl 4'-hydroxybiphenyl-4-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:
Guidance literature:
Multi-step reaction with 4 steps
1: K2CO3 / acetone
2: Mg, C2H5Br / diethyl ether
3: 48percent HBr / acetic acid
4: H(+) / toluene
With ethyl bromide; hydrogen bromide; hydrogen cation; potassium carbonate; magnesium; In diethyl ether; acetic acid; acetone; toluene;
Guidance literature:
4-iodobenzoic acid; dodecyl 4'-hydroxybiphenyl-4-carboxylate; With dicyclohexyl-carbodiimide; dmap; In dichloromethane; for 24h;
In dichloromethane; for 4h; Heating;
DOI:10.1080/15421400490425784
Guidance literature:
Multi-step reaction with 2 steps
1.1: DCC / DMAP / CH2Cl2 / 24 h
1.2: 45.8 percent / CH2Cl2 / 4 h / Heating
2.1: 45 percent / (i-Pr)2NH / PdCl2(Ph3P)2; CuI / tetrahydrofuran / 48 h
With diisopropylamine; dicyclohexyl-carbodiimide; dmap; bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; In tetrahydrofuran; dichloromethane;
DOI:10.1080/15421400490425784
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