Benzoic acid 1-[3,3,3-trifluoro-2-(tetrahydro-pyran-2-yloxy)-propyl]-but-3-enyl ester

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Chemical Name:Benzoic acid 1-[3,3,3-trifluoro-2-(tetrahydro-pyran-2-yloxy)-propyl]-but-3-enyl ester
CAS No.:155226-12-3
Molecular Formula:C₁₉H₂₃F₃O₄
Molecular Weight:372.384
Hs Code.:

Synonyms:Benzoic acid 1-[3,3,3-trifluoro-2-(tetrahydro-pyran-2-yloxy)-propyl]-but-3-enyl ester

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Chemical Property of Benzoic acid 1-[3,3,3-trifluoro-2-(tetrahydro-pyran-2-yloxy)-propyl]-but-3-enyl ester

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Technology Process of Benzoic acid 1-[3,3,3-trifluoro-2-(tetrahydro-pyran-2-yloxy)-propyl]-but-3-enyl ester

There total 4 articles about Benzoic acid 1-[3,3,3-trifluoro-2-(tetrahydro-pyran-2-yloxy)-propyl]-but-3-enyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 142435-84-5,108535-31-5,111056-68-9
4,4,4-trifluoro-3-tetrahydropyranyloxybutyl alcohol

: 155226-12-3
Benzoic acid 1-[3,3,3-trifluoro-2-(tetrahydro-pyran-2-yloxy)-propyl]-but-3-enyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: pyridinium chlorochromate, AcONa / CH₂Cl₂ / 3 h / Ambient temperature

2: 1.) Mg / 2.) ether, r.t., 1.5 h

3: pyridine / 1.5 h / Ambient temperature

With pyridine; sodium acetate; magnesium; pyridinium chlorochromate; In dichloromethane;
DOI:10.1016/S0022-1139(00)80477-7

Reference yield:

: 142435-83-4,108535-30-4
ethyl 4,4,4-trifluoro-3-tetrahydropyranyloxybutyrate

: 155226-12-3
Benzoic acid 1-[3,3,3-trifluoro-2-(tetrahydro-pyran-2-yloxy)-propyl]-but-3-enyl ester

Guidance literature:: Multi-step reaction with 4 steps

1: LiAlH₄ / diethyl ether / 1 h / 0 °C

2: pyridinium chlorochromate, AcONa / CH₂Cl₂ / 3 h / Ambient temperature

3: 1.) Mg / 2.) ether, r.t., 1.5 h

4: pyridine / 1.5 h / Ambient temperature

With pyridine; lithium aluminium tetrahydride; sodium acetate; magnesium; pyridinium chlorochromate; In diethyl ether; dichloromethane;
DOI:10.1016/S0022-1139(00)80477-7

Reference yield:

: 108535-34-8
4,4,4-Trifluoro-3-(tetrahydro-pyran-2-yloxy)-butyraldehyde

: 155226-12-3
Benzoic acid 1-[3,3,3-trifluoro-2-(tetrahydro-pyran-2-yloxy)-propyl]-but-3-enyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) Mg / 2.) ether, r.t., 1.5 h

2: pyridine / 1.5 h / Ambient temperature

With pyridine; magnesium;
DOI:10.1016/S0022-1139(00)80477-7