C₁₉H₂₁Cl₃N₂O*ClH

Base Information

Chemical Name:C₁₉H₂₁Cl₃N₂O*ClH
CAS No.:1622845-98-0
Molecular Formula:C₁₉H₂₁Cl₃N₂O*ClH
Molecular Weight:436.208
Hs Code.:

C<sub>19</sub>H<sub>21</sub>Cl<sub>3</sub>N<sub>2</sub>O*ClH

Synonyms:C₁₉H₂₁Cl₃N₂O*ClH

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₁₉H₂₁Cl₃N₂O*ClH

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Technology Process of C₁₉H₂₁Cl₃N₂O*ClH

There total 6 articles about C₁₉H₂₁Cl₃N₂O*ClH which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 1188535-40-1
C₂₄H₂₉Cl₃N₂O₃

: 1622845-98-0
C₁₉H₂₁Cl₃N₂O*ClH

Guidance literature:: With hydrogenchloride; In ethyl acetate; at 20 ℃;
DOI:10.1016/j.bmcl.2014.06.046

Reference yield:

: 95-76-1
m,p-dichloroaniline

: 1622845-98-0
C₁₉H₂₁Cl₃N₂O*ClH

Guidance literature:: Multi-step reaction with 6 steps

1: potassium phosphate; copper(I) bromide / N,N-dimethyl-formamide / 40 - 50 °C

2: triethylamine; C₆H₅N₃O*C₈H₁₇N₃ / N,N-dimethyl-formamide / 20 °C

3: lithium aluminium tetrahydride / tetrahydrofuran / 50 °C

4: tetrahydrofuran / 20 °C

5: triethylamine / tetrahydrofuran / 60 °C

6: hydrogenchloride / ethyl acetate / 20 °C

With hydrogenchloride; potassium phosphate; lithium aluminium tetrahydride; C₆H₅N₃O*C₈H₁₇N₃; triethylamine; copper(I) bromide; In tetrahydrofuran; ethyl acetate; N,N-dimethyl-formamide; 1: |Ullmann Condensation;
DOI:10.1016/j.bmcl.2014.06.046

Reference yield:

: 34129-52-7
3-(3,4-dichloroanilino)-butyric acid

: 1622845-98-0
C₁₉H₂₁Cl₃N₂O*ClH

Guidance literature:: Multi-step reaction with 5 steps

1: triethylamine; C₆H₅N₃O*C₈H₁₇N₃ / N,N-dimethyl-formamide / 20 °C

2: lithium aluminium tetrahydride / tetrahydrofuran / 50 °C

3: tetrahydrofuran / 20 °C

4: triethylamine / tetrahydrofuran / 60 °C

5: hydrogenchloride / ethyl acetate / 20 °C

With hydrogenchloride; lithium aluminium tetrahydride; C₆H₅N₃O*C₈H₁₇N₃; triethylamine; In tetrahydrofuran; ethyl acetate; N,N-dimethyl-formamide;
DOI:10.1016/j.bmcl.2014.06.046