3,4,5-trichlorobenzylamine

Base Information

• Chemical Name: 3,4,5-trichlorobenzylamine
• CAS No.: 101084-07-5
• Molecular Formula: C₇H₆Cl₃N
• Molecular Weight: 210.49

Synonyms:3,4,5-trichlorobenzylamine

Chemical Property of 3,4,5-trichlorobenzylamine

Chemical Property:

Purity/Quality:

3,4,5-Trichlorobenzylamine ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
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MSDS Files:

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Technology Process of 3,4,5-trichlorobenzylamine

There total 1 articles about 3,4,5-trichlorobenzylamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

3,4,5-trichloro-toluene (21472-86-6) → 3,4,5-trichlorobenzylamine (101084-07-5)

Guidance literature:

Multistep reaction; (i) Br₂, (heating), (ii) hexamethylenetetramine;

Reference yield: 83.0%

thiophosgene (463-71-8) + 3,4,5-trichlorobenzylamine (101084-07-5) → 3,4,5-trichlorobenzyl isothiocyanate

Guidance literature:

With sodium hydrogencarbonate; In dichloromethane; water; at 20 ℃; for 15h;

DOI:10.1016/j.bmc.2016.10.015

Reference yield:

3,4,5-trichlorobenzylamine (101084-07-5) → (2S,3S,4S,5S)-N-(3,4,5-trichlorobenzyl)-3,4-dihydroxy-2,5-bis(hydroxymethyl)pyrrolidine-1-carbothioamide

Guidance literature:

Multi-step reaction with 2 steps

1: sodium hydrogencarbonate / water; dichloromethane / 15 h / 20 °C

2: triethylamine / pyridine / 21 h / 20 °C

With sodium hydrogencarbonate; triethylamine; In pyridine; dichloromethane; water;

DOI:10.1016/j.bmc.2016.10.015

upstream raw materials:

3,4,5-trichloro-toluene

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