C₄₅H₇₉IO₁₀SSi₂

Base Information

Chemical Name:C₄₅H₇₉IO₁₀SSi₂
CAS No.:1316279-24-9
Molecular Formula:C₄₅H₇₉IO₁₀SSi₂
Molecular Weight:995.258
Hs Code.:

C<sub>45</sub>H<sub>79</sub>IO<sub>10</sub>SSi<sub>2</sub>

Synonyms:C₄₅H₇₉IO₁₀SSi₂

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₄₅H₇₉IO₁₀SSi₂

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Technology Process of C₄₅H₇₉IO₁₀SSi₂

There total 24 articles about C₄₅H₇₉IO₁₀SSi₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

: 1316278-94-0
C₅₀H₈₇IO₁₁SSi₂

: 1316279-24-9
C₄₅H₇₉IO₁₀SSi₂

Guidance literature:: With methanol; sodium methylate; In tetrahydrofuran; at 20 ℃; for 1h;

Reference yield:

: 1139773-78-6
C₁₆H₂₅NO₅

: 1316279-24-9
C₄₅H₇₉IO₁₀SSi₂

Guidance literature:: Multi-step reaction with 13 steps

1.1: 1H-imidazole / N,N-dimethyl-formamide / 2 h / 0 - 20 °C

2.1: lithium borohydride / tetrahydrofuran / 16 h / 0 - 23 °C

2.2: 0.5 h / 0 - 10 °C

3.1: dmap; triethylamine / dichloromethane / 2 h / 0 - 22 °C

4.1: zinc / methanesulfonic acid / tetrahydrofuran / 5 h / Reflux

5.1: water; acetic acid / tetrahydrofuran / 10 h / 10 - 20 °C

6.1: hydrogen / palladium 10% on activated carbon / ethyl acetate / 2 h / 20 °C

7.1: toluene / 0.25 h / 95 °C

8.1: potassium hexamethylsilazane / toluene; tetrahydrofuran / 1 h / -30 - -25 °C

9.1: hydrogenchloride / isopropyl alcohol; methanol / 1 h / 20 °C

10.1: pyridine / dichloromethane / 1 h / -10 - 0 °C

11.1: sodium iodide / dichloromethane; N,N-dimethyl-formamide / 3 h / 20 - 22 °C

12.1: triethylamine; nickel dichloride; chromium dichloride; (S)-N-(2-(4-isopropyl-4,5-dihydrooxazol-2-yl)-6-methylphenyl)methane sulfonamide / tetrahydrofuran / 20.5 h / 22 - 24 °C / Inert atmosphere

12.2: 1 h / 0 - 5 °C

13.1: sodium methylate; methanol / tetrahydrofuran / 1 h / 20 °C

With pyridine; 1H-imidazole; chromium dichloride; hydrogenchloride; methanol; dmap; lithium borohydride; water; hydrogen; sodium methylate; potassium hexamethylsilazane; acetic acid; triethylamine; sodium iodide; nickel dichloride; zinc; (S)-N-(2-(4-isopropyl-4,5-dihydrooxazol-2-yl)-6-methylphenyl)methane sulfonamide; methanesulfonic acid; palladium 10% on activated carbon; In tetrahydrofuran; methanol; dichloromethane; ethyl acetate; N,N-dimethyl-formamide; isopropyl alcohol; toluene; 12.1: Nozaki-Hiyama-Kishi Coupling;

Reference yield:

: 1316278-79-1
C₂₆H₄₇NO₅Si

: 1316279-24-9
C₄₅H₇₉IO₁₀SSi₂

Guidance literature:: Multi-step reaction with 10 steps

1.1: zinc / methanesulfonic acid / tetrahydrofuran / 5 h / Reflux

2.1: water; acetic acid / tetrahydrofuran / 10 h / 10 - 20 °C

3.1: hydrogen / palladium 10% on activated carbon / ethyl acetate / 2 h / 20 °C

4.1: toluene / 0.25 h / 95 °C

5.1: potassium hexamethylsilazane / toluene; tetrahydrofuran / 1 h / -30 - -25 °C

6.1: hydrogenchloride / isopropyl alcohol; methanol / 1 h / 20 °C

7.1: pyridine / dichloromethane / 1 h / -10 - 0 °C

8.1: sodium iodide / dichloromethane; N,N-dimethyl-formamide / 3 h / 20 - 22 °C

9.1: triethylamine; nickel dichloride; chromium dichloride; (S)-N-(2-(4-isopropyl-4,5-dihydrooxazol-2-yl)-6-methylphenyl)methane sulfonamide / tetrahydrofuran / 20.5 h / 22 - 24 °C / Inert atmosphere

9.2: 1 h / 0 - 5 °C

10.1: sodium methylate; methanol / tetrahydrofuran / 1 h / 20 °C

With pyridine; chromium dichloride; hydrogenchloride; methanol; water; hydrogen; sodium methylate; potassium hexamethylsilazane; acetic acid; triethylamine; sodium iodide; nickel dichloride; zinc; (S)-N-(2-(4-isopropyl-4,5-dihydrooxazol-2-yl)-6-methylphenyl)methane sulfonamide; methanesulfonic acid; palladium 10% on activated carbon; In tetrahydrofuran; methanol; dichloromethane; ethyl acetate; N,N-dimethyl-formamide; isopropyl alcohol; toluene; 9.1: Nozaki-Hiyama-Kishi Coupling;