phenylmethyl 3-O-(tert-butyldimethylsilyl)-4-O-[3-O-[α-L-rhodinopyranosyl]-4-O-(tert-butyldimethylsilyl)-β-D-olivopyranosyl]-β-D-olivopyranoside

Base Information

• Chemical Name: phenylmethyl 3-O-(tert-butyldimethylsilyl)-4-O-[3-O-[α-L-rhodinopyranosyl]-4-O-(tert-butyldimethylsilyl)-β-D-olivopyranosyl]-β-D-olivopyranoside
• CAS No.: 1030632-60-0
• Molecular Formula: C₃₇H₆₆O₉Si₂
• Molecular Weight: 711.097

Synonyms:phenylmethyl 3-O-(tert-butyldimethylsilyl)-4-O-[3-O-[α-L-rhodinopyranosyl]-4-O-(tert-butyldimethylsilyl)-β-D-olivopyranosyl]-β-D-olivopyranoside

Chemical Property of phenylmethyl 3-O-(tert-butyldimethylsilyl)-4-O-[3-O-[α-L-rhodinopyranosyl]-4-O-(tert-butyldimethylsilyl)-β-D-olivopyranosyl]-β-D-olivopyranoside

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Technology Process of phenylmethyl 3-O-(tert-butyldimethylsilyl)-4-O-[3-O-[α-L-rhodinopyranosyl]-4-O-(tert-butyldimethylsilyl)-β-D-olivopyranosyl]-β-D-olivopyranoside

There total 1 articles about phenylmethyl 3-O-(tert-butyldimethylsilyl)-4-O-[3-O-[α-L-rhodinopyranosyl]-4-O-(tert-butyldimethylsilyl)-β-D-olivopyranosyl]-β-D-olivopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

phenylmethyl 3-O-(tert-butyldimethylsilyl)-4-O-[3-O-[(2S,5S,6S)-5,6-dihydro-5-hydroxy-6-methyl-2H-pyran-2-yl]-4-O-(tert-butyldimethylsilyl)-β-D-olivopyranosyl]-β-D-olivopyranoside (1030632-58-6) → phenylmethyl 3-O-(tert-butyldimethylsilyl)-4-O-[3-O-[α-L-rhodinopyranosyl]-4-O-(tert-butyldimethylsilyl)-β-D-olivopyranosyl]-β-D-olivopyranoside (1030632-60-0)

Guidance literature:

With 2-nitrobenzenesulfonyl hydrazide; triethylamine; In dichloromethane; at 20 ℃; for 12h; Inert atmosphere;

DOI:10.1021/ol800697k

Reference yield: 97.0%

phenylmethyl 3-O-(tert-butyldimethylsilyl)-4-O-[3-O-[α-L-rhodinopyranosyl]-4-O-(tert-butyldimethylsilyl)-β-D-olivopyranosyl]-β-D-olivopyranoside (1030632-60-0) → phenylmethyl 4-O-[3-O-[α-L-rhodinopyranosyl]-β-D-olivopyranosyl]-β-D-olivopyranoside (1030632-61-1)

Guidance literature:

With tetrabutyl ammonium fluoride; In tetrahydrofuran; at 20 ℃; for 5h;

DOI:10.1021/ol800697k

upstream raw materials:

phenylmethyl 3-O-(tert-butyldimethylsilyl)-4-O-[3-O-[(2S,5S,6S)-5,6-dihydro-5-hydroxy-6-methyl-2H-pyran-2-yl]-4-O-(tert-butyldimethylsilyl)-β-D-olivopyranosyl]-β-D-olivopyranoside

Downstream raw materials:

phenylmethyl 4-O-[3-O-[α-L-rhodinopyranosyl]-β-D-olivopyranosyl]-β-D-olivopyranoside

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