(2R,3S,4S)-2,4,5-tris(p-methoxybenzyloxy)-1,3-O-sulfonylpentane-1,3-diol

Base Information

Chemical Name:(2R,3S,4S)-2,4,5-tris(p-methoxybenzyloxy)-1,3-O-sulfonylpentane-1,3-diol
CAS No.:1101107-60-1
Molecular Formula:C₂₉H₃₄O₁₀S
Molecular Weight:574.649
Hs Code.:

Synonyms:(2R,3S,4S)-2,4,5-tris(p-methoxybenzyloxy)-1,3-O-sulfonylpentane-1,3-diol

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (2R,3S,4S)-2,4,5-tris(p-methoxybenzyloxy)-1,3-O-sulfonylpentane-1,3-diol

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Technology Process of (2R,3S,4S)-2,4,5-tris(p-methoxybenzyloxy)-1,3-O-sulfonylpentane-1,3-diol

There total 1 articles about (2R,3S,4S)-2,4,5-tris(p-methoxybenzyloxy)-1,3-O-sulfonylpentane-1,3-diol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₂₉H₃₄O₉S

: 1101107-60-1
(2R,3S,4S)-2,4,5-tris(p-methoxybenzyloxy)-1,3-O-sulfonylpentane-1,3-diol

Guidance literature:: With sodium periodate; In tetrachloromethane; water; acetonitrile; at 0 ℃; for 1h; Inert atmosphere;

Reference yield: 80.0%

: 1101107-60-1
(2R,3S,4S)-2,4,5-tris(p-methoxybenzyloxy)-1,3-O-sulfonylpentane-1,3-diol

: 630108-94-0
N-tert-butoxycarbonyl-L-homocysteine tert-butyl ester

: 1101107-61-2
2(S)-tert-butoxycarbonylamino-4-[(2S,3R,4S)-3-hydroxy-2,4,5-tris(p-methoxybenzyloxy)-pentylsulfanyl]-butyric acid tert-butyl ester

Guidance literature:: N-tert-butoxycarbonyl-L-homocysteine tert-butyl ester; With n-butyllithium; In hexane; N,N-dimethyl-formamide; at 0 ℃; for 0.0833333h; Inert atmosphere;

(2R,3S,4S)-2,4,5-tris(p-methoxybenzyloxy)-1,3-O-sulfonylpentane-1,3-diol; In hexane; N,N-dimethyl-formamide; at 0 - 20 ℃; for 4h; Inert atmosphere;

With sulfuric acid; In tetrahydrofuran; water; at 0 ℃; for 1h; Inert atmosphere;