(Z)-(4-tert-butylphenyl)-2-bromovinyl acetate

Base Information

• Chemical Name: (Z)-(4-tert-butylphenyl)-2-bromovinyl acetate
• CAS No.: 1233843-42-9
• Molecular Formula: C₁₄H₁₇BrO₂
• Molecular Weight: 297.192
• Mol file: 1233843-42-9.mol

Synonyms:(Z)-(4-tert-butylphenyl)-2-bromovinyl acetate

Chemical Property of (Z)-(4-tert-butylphenyl)-2-bromovinyl acetate

Chemical Property:

Purity/Quality:

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Technology Process of (Z)-(4-tert-butylphenyl)-2-bromovinyl acetate

There total 1 articles about (Z)-(4-tert-butylphenyl)-2-bromovinyl acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

4-tert-Butylphenylacetylene (772-38-3) + acetic anhydride (108-24-7) → (Z)-(4-tert-butylphenyl)-2-bromovinyl acetate (1233843-42-9)

Guidance literature:

With N-Bromosuccinimide; silver tetrafluoroborate; at 120 ℃; for 12h; stereoselective reaction;

DOI:10.1021/ol101251n

Reference yield: 83.0%

(Z)-(4-tert-butylphenyl)-2-bromovinyl acetate (1233843-42-9) → 2,5-bis(4-t-butylphenyl)pyrazine (1458055-88-3)

Guidance literature:

With ammonium formate; In N,N-dimethyl-formamide; at 120 ℃; for 6h; regioselective reaction; Schlenk technique;

DOI:10.1039/c3ob41164h

upstream raw materials:

4-tert-Butylphenylacetylene

acetic anhydride

Downstream raw materials:

2,5-bis(4-t-butylphenyl)pyrazine