2,3,6-tri-O-benzoyl-4-O-trifluoromethylsulfonyl-α-D-glucopyranosyl-(1<*>1)-2,3,6-tri-O-benzoyl-4-O-trifluoromethylsulfonyl-α-D-glucopyranoside

Base Information

• Chemical Name: 2,3,6-tri-O-benzoyl-4-O-trifluoromethylsulfonyl-α-D-glucopyranosyl-(1<*>1)-2,3,6-tri-O-benzoyl-4-O-trifluoromethylsulfonyl-α-D-glucopyranoside
• CAS No.: 173543-50-5
• Molecular Formula: C₅₆H₄₄F₆O₂₁S₂
• Molecular Weight: 1231.08
• Mol file: 173543-50-5.mol

Synonyms:2,3,6-tri-O-benzoyl-4-O-trifluoromethylsulfonyl-α-D-glucopyranosyl-(1<*>1)-2,3,6-tri-O-benzoyl-4-O-trifluoromethylsulfonyl-α-D-glucopyranoside

Chemical Property of 2,3,6-tri-O-benzoyl-4-O-trifluoromethylsulfonyl-α-D-glucopyranosyl-(1<*>1)-2,3,6-tri-O-benzoyl-4-O-trifluoromethylsulfonyl-α-D-glucopyranoside

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 2,3,6-tri-O-benzoyl-4-O-trifluoromethylsulfonyl-α-D-glucopyranosyl-(1<*>1)-2,3,6-tri-O-benzoyl-4-O-trifluoromethylsulfonyl-α-D-glucopyranoside

There total 1 articles about 2,3,6-tri-O-benzoyl-4-O-trifluoromethylsulfonyl-α-D-glucopyranosyl-(1<*>1)-2,3,6-tri-O-benzoyl-4-O-trifluoromethylsulfonyl-α-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2,3,6-tri-O-benzoyl-α-D-glucopyranosyl-(1<*>1)-2,3,6-tri-O-benzoyl-α-D-glucopyranoside (64244-20-8) + trifluoromethylsulfonic anhydride (358-23-6) → 2,3,6-tri-O-benzoyl-4-O-trifluoromethylsulfonyl-α-D-glucopyranosyl-(1<*>1)-2,3,6-tri-O-benzoyl-4-O-trifluoromethylsulfonyl-α-D-glucopyranoside (173543-50-5)

Guidance literature:

With pyridine; In dichloromethane; at 0 - 20 ℃;

DOI:10.1016/0008-6215(95)00226-J

Reference yield: 75.0%

2,3,6-tri-O-benzoyl-4-O-trifluoromethylsulfonyl-α-D-glucopyranosyl-(1<*>1)-2,3,6-tri-O-benzoyl-4-O-trifluoromethylsulfonyl-α-D-glucopyranoside (173543-50-5) → 4-azido-2,3,6-tri-O-benzoyl-4-deoxy-α-D-galactopyranosyl-(1<*>1)-4-azido-2,3,6-tri-O-benzoyl-4-deoxy-α-D-galactopyranoside

Guidance literature:

With sodium azide; dicyclopentano-15-crown-5; In N,N-dimethyl-formamide; at 60 ℃; for 5h;

DOI:10.1016/0008-6215(95)00226-J

Reference yield: 72.0%

2,3,6-tri-O-benzoyl-4-O-trifluoromethylsulfonyl-α-D-glucopyranosyl-(1<*>1)-2,3,6-tri-O-benzoyl-4-O-trifluoromethylsulfonyl-α-D-glucopyranoside (173543-50-5) → 2,3,6-tri-O-benzoyl-α-D-galactopyranosyl-(1<*>1)-2,3,6-tri-O-benzoyl-α-D-galactopyranoside

Guidance literature:

With sodium nitrite; In N,N-dimethyl-formamide; for 1h; Ambient temperature;

DOI:10.1016/0008-6215(95)00226-J

upstream raw materials:

2,3,6-tri-O-benzoyl-α-D-glucopyranosyl-(1<*>1)-2,3,6-tri-O-benzoyl-α-D-glucopyranoside

trifluoromethylsulfonic anhydride