(2S,3S)-2-Benzyloxymethyl-3-hydroxy-butyric acid methyl ester

Base Information

Chemical Name:(2S,3S)-2-Benzyloxymethyl-3-hydroxy-butyric acid methyl ester
CAS No.:121793-81-5
Molecular Formula:C₁₃H₁₈O₄
Molecular Weight:238.284
Hs Code.:

Synonyms:(2S,3S)-2-Benzyloxymethyl-3-hydroxy-butyric acid methyl ester

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Chemical Property of (2S,3S)-2-Benzyloxymethyl-3-hydroxy-butyric acid methyl ester

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Technology Process of (2S,3S)-2-Benzyloxymethyl-3-hydroxy-butyric acid methyl ester

There total 2 articles about (2S,3S)-2-Benzyloxymethyl-3-hydroxy-butyric acid methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 3587-60-8
Benzyloxymethyl chloride

: 3976-69-0
Methyl (R)-3-hydroxybutyrate

: 107441-54-3,121793-81-5
(3R)-methyl 2-<(benzyloxy)methyl>-3-hydroxybutyrate

Guidance literature:: With lithium diisopropyl amide; Yield given. Multistep reaction; 1.) THF, 55 min, 2.) THF, 0 deg C, 4 h;
DOI:10.1021/jo00385a024

Reference yield:

: 53562-86-0
(S)-3-hydroxybutyric acid methyl ester

: 121793-81-5
(2S,3S)-2-Benzyloxymethyl-3-hydroxy-butyric acid methyl ester

Guidance literature:: DOI:10.1039/c39880001202

Reference yield: 88.0%

: 58479-61-1
tert-butylchlorodiphenylsilane

: 121793-81-5
(2S,3S)-2-Benzyloxymethyl-3-hydroxy-butyric acid methyl ester

: (2S,3S)-methyl 2-(benzyloxymethyl)-3-(tert-butyldiphenylsilyloxy)butanoate

Guidance literature:: (2S,3S)-2-Benzyloxymethyl-3-hydroxy-butyric acid methyl ester; With 1H-imidazole; dmap; In dichloromethane; for 0.25h;

tert-butylchlorodiphenylsilane; In dichloromethane; at 0 - 20 ℃;
DOI:10.1016/j.tetlet.2014.11.109