3β-cholestanyl 2,3,4-tri-O-benzyl-α-L-rhamnopyranoside

Base Information

Chemical Name:3β-cholestanyl 2,3,4-tri-O-benzyl-α-L-rhamnopyranoside
CAS No.:129796-69-6
Molecular Formula:C₅₄H₇₆O₅
Molecular Weight:805.194
Hs Code.:

Synonyms:3β-cholestanyl 2,3,4-tri-O-benzyl-α-L-rhamnopyranoside

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Chemical Property of 3β-cholestanyl 2,3,4-tri-O-benzyl-α-L-rhamnopyranoside

Chemical Property:

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Technology Process of 3β-cholestanyl 2,3,4-tri-O-benzyl-α-L-rhamnopyranoside

There total 4 articles about 3β-cholestanyl 2,3,4-tri-O-benzyl-α-L-rhamnopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 80-97-7
Cholestanol

: 2,3,4-tri-O-benzyl-6-deoxy-L-mannopyranosyl dimethylphosphinothioate

: 129796-69-6
3β-cholestanyl 2,3,4-tri-O-benzyl-α-L-rhamnopyranoside

Guidance literature:: With 4 A molecular sieve; trityl perchlorate; iodine; In benzene; Ambient temperature;
DOI:10.1246/bcsj.67.1359

Reference yield:

: 80-97-7
Cholestanol

: 131897-04-6
phenyl 2,3,4-tri-O-benzyl-1-thio-α-L-rhamnopyranoside

: 129796-69-6
3β-cholestanyl 2,3,4-tri-O-benzyl-α-L-rhamnopyranoside

: 129796-70-9
3β-cholestanyl 2,3,4-tri-O-benzyl-β-L-rhamnopyranoside

Guidance literature:: phenyl 2,3,4-tri-O-benzyl-1-thio-α-L-rhamnopyranoside; With 1-benzenesulfinyl piperidine; trifluoromethylsulfonic anhydride; 2,4,6-tri-tert-butylpyrimidine; In dichloromethane; at -60 ℃; for 0.333333h;

Cholestanol; In dichloromethane; at -60 ℃; for 1h;
DOI:10.1021/jo035003j

Reference yield:

: 80-97-7
Cholestanol

: 2,3,4-tri-O-benzyl-6-deoxy-L-mannopyranosyl dimethylphosphinothioate

: 129796-69-6
3β-cholestanyl 2,3,4-tri-O-benzyl-α-L-rhamnopyranoside

: 129796-70-9
3β-cholestanyl 2,3,4-tri-O-benzyl-β-L-rhamnopyranoside

Guidance literature:: With 4 A molecular sieve; trityl perchlorate; iodine; In fluorobenzene; Yield given. Yields of byproduct given. Title compound not separated from byproducts; Ambient temperature;
DOI:10.1246/bcsj.67.1359