Potassium (3-aminophenyl)trifluoroboranuide

Base Information

• Chemical Name: Potassium (3-aminophenyl)trifluoroboranuide
• CAS No.: 1160186-73-1
• Molecular Formula: C₆H₆BF₃N*K
• Molecular Weight: 199.025
• Hs Code.: 2932190090
• Mol file: 1160186-73-1.mol

Synonyms:potassium 3-aminophenyltrifluoroborate

Chemical Property of Potassium (3-aminophenyl)trifluoroboranuide

Chemical Property:

• Melting Point: >186°C (dec.)
• Storage Temp.: Hygroscopic, -20°C Freezer, Under inert atmosphere
• Solubility.: DMSO (Sparingly), Methanol (Slightly)

Purity/Quality:

98% ^*data from raw suppliers

Potassium(3-Aminophenyl)trifluoroborate ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of Potassium (3-aminophenyl)trifluoroboranuide

There total 1 articles about Potassium (3-aminophenyl)trifluoroboranuide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

3-Aminophenylboronic acid (30418-59-8,280563-63-5) → potassium 3-aminophenyltrifluoroborate (1160186-73-1)

Guidance literature:

3-Aminophenylboronic acid; With potassium fluoride; In water; acetonitrile; at 21 ℃;

With L-Tartaric acid; In tetrahydrofuran; water; acetonitrile;

DOI:10.1002/anie.201203930

Reference yield: 78.0%

potassium 3-aminophenyltrifluoroborate (1160186-73-1) + water (7732-18-5) → 3-Aminophenylboronic acid (30418-59-8,280563-63-5)

Guidance literature:

With montmorillonite K₁₀; at 25 ℃; for 1.5h;

DOI:10.21577/0103-5053.20180126

Reference yield: 73.0%

potassium 3-aminophenyltrifluoroborate (1160186-73-1) + anthranilic acid amide (28144-70-9,88-68-6) → 2-(3-aminophenyl)-1,3,2-benzodiazaborininone

Guidance literature:

With boron trifluoride monoethylamine; In toluene; at 80 ℃; for 16h; Inert atmosphere; Sealed tube;

DOI:10.1021/acs.joc.7b00747

upstream raw materials:

3-Aminophenylboronic acid

Downstream raw materials:

3-Aminophenylboronic acid

Refernces