2-Phenyl-butyric acid (4bR,10bS,11S)-10b-hydroxy-5-methyl-4b,5,6,10b,11,12-hexahydro-benzo[c]phenanthridin-11-yl ester

Base Information

Chemical Name:2-Phenyl-butyric acid (4bR,10bS,11S)-10b-hydroxy-5-methyl-4b,5,6,10b,11,12-hexahydro-benzo[c]phenanthridin-11-yl ester
CAS No.:82884-88-6
Molecular Formula:C₂₈H₂₉NO₃
Molecular Weight:427.543
Hs Code.:

Synonyms:2-Phenyl-butyric acid (4bR,10bS,11S)-10b-hydroxy-5-methyl-4b,5,6,10b,11,12-hexahydro-benzo[c]phenanthridin-11-yl ester

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Chemical Property of 2-Phenyl-butyric acid (4bR,10bS,11S)-10b-hydroxy-5-methyl-4b,5,6,10b,11,12-hexahydro-benzo[c]phenanthridin-11-yl ester

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Technology Process of 2-Phenyl-butyric acid (4bR,10bS,11S)-10b-hydroxy-5-methyl-4b,5,6,10b,11,12-hexahydro-benzo[c]phenanthridin-11-yl ester

There total 4 articles about 2-Phenyl-butyric acid (4bR,10bS,11S)-10b-hydroxy-5-methyl-4b,5,6,10b,11,12-hexahydro-benzo[c]phenanthridin-11-yl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 1519-21-7
2-phenylbutyric anhydride

: 81370-45-8
(+)-(4bR,10bS,11S)-4b,5,6,10b,11,12-hexahydro-10b,11-dihydroxy-5-methylbenzophenanthridine

: 90-27-7
2-Phenylbutyric acid

: 82884-88-6
2-Phenyl-butyric acid (4bR,10bS,11S)-10b-hydroxy-5-methyl-4b,5,6,10b,11,12-hexahydro-benzo[c]phenanthridin-11-yl ester

Guidance literature:: With pyridine; for 17h; Ambient temperature;

Reference yield:

: 81370-44-7
(+)-(4bR,10bS,11S,12S)-4b,5,6,10b,11,12-hexahydro-10b,11,12-trihydroxy-5-methylbenzophenanthridine

: 82884-88-6
2-Phenyl-butyric acid (4bR,10bS,11S)-10b-hydroxy-5-methyl-4b,5,6,10b,11,12-hexahydro-benzo[c]phenanthridin-11-yl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 78 percent / 70percentHClO₄, H₂ / aq. HCl / 66 h / 70 °C / 3800 Torr

2: 90 percent / pyridine / 17 h / Ambient temperature

With pyridine; perchloric acid; hydrogen; In hydrogenchloride;

Reference yield:

: 77199-05-4
C₁₇H₁₂O₄

: 82884-88-6
2-Phenyl-butyric acid (4bR,10bS,11S)-10b-hydroxy-5-methyl-4b,5,6,10b,11,12-hexahydro-benzo[c]phenanthridin-11-yl ester

Guidance literature:: Multi-step reaction with 4 steps

1: 99 percent / 1 h / Ambient temperature

2: 99 percent / LiAlH₄, AlCl₃ / 1,2-dimethoxy-ethane / 1.5 h / Heating

3: 78 percent / 70percentHClO₄, H₂ / aq. HCl / 66 h / 70 °C / 3800 Torr

4: 90 percent / pyridine / 17 h / Ambient temperature

With pyridine; lithium aluminium tetrahydride; aluminium trichloride; perchloric acid; hydrogen; In hydrogenchloride; 1,2-dimethoxyethane;