N,N-[[(2-methylpyridine)imino]di-1,2-ethandiyl]bis(4-methylbenzenesulfonamide)

Base Information

Chemical Name:N,N-[[(2-methylpyridine)imino]di-1,2-ethandiyl]bis(4-methylbenzenesulfonamide)
CAS No.:406911-13-5
Molecular Formula:C₂₄H₃₀N₄O₄S₂
Molecular Weight:502.659
Hs Code.:

Synonyms:N,N-[[(2-methylpyridine)imino]di-1,2-ethandiyl]bis(4-methylbenzenesulfonamide)

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N,N-[[(2-methylpyridine)imino]di-1,2-ethandiyl]bis(4-methylbenzenesulfonamide)

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Technology Process of N,N-[[(2-methylpyridine)imino]di-1,2-ethandiyl]bis(4-methylbenzenesulfonamide)

There total 2 articles about N,N-[[(2-methylpyridine)imino]di-1,2-ethandiyl]bis(4-methylbenzenesulfonamide) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 3731-51-9
2-(Aminomethyl)pyridine

: 3634-89-7
N-(p-toluenesulfonyl)aziridine

: 406911-13-5
N,N-[[(2-methylpyridine)imino]di-1,2-ethandiyl]bis(4-methylbenzenesulfonamide)

Guidance literature:: In ethanol;
DOI:10.1016/j.poly.2021.115552

Reference yield:

: 98-59-9
p-toluenesulfonyl chloride

: 406911-13-5
N,N-[[(2-methylpyridine)imino]di-1,2-ethandiyl]bis(4-methylbenzenesulfonamide)

Guidance literature:: Multi-step reaction with 2 steps

1: potassium hydroxide / dichloromethane

2: ethanol

With potassium hydroxide; In ethanol; dichloromethane;
DOI:10.1016/j.poly.2021.115552

Reference yield: 68.0%

: indium (III) tris(hexamethyldisilyl) amide

: 406911-13-5
N,N-[[(2-methylpyridine)imino]di-1,2-ethandiyl]bis(4-methylbenzenesulfonamide)

: 1269621-53-5
[In(N(SiMe₃)2)((2-NC₅H₄)CH₂N(CH₂CH₂NTs)2)]

Guidance literature:: In toluene; (Ar or N2); using Schlenk techniques; addn. dropwise of soln. of C5H4NCH2N(CH2CH2NHTs)2 in toluene to soln. of In(N(SiMe3)2)3 in toluene at roomtemp., heating at 70°C for 48 h; removal of volatiles under reduced pressure, addn. of hexanes, filtration, washing with THF, drying in vac., dissolving in CH2Cl2; layering withhexanes, crystn., drying in vac.; elem. anal.;
DOI:10.1021/om101166s