2,9,9-Trimethyl-4-(2,9,9-trimethyl-3,5-dioxa-4-boratricyclo[6.1.1.02,6]decan-4-yl)-3,5-dioxa-4-boratricyclo[6.1.1.02,6]decane

Base Information

Chemical Name:2,9,9-Trimethyl-4-(2,9,9-trimethyl-3,5-dioxa-4-boratricyclo[6.1.1.02,6]decan-4-yl)-3,5-dioxa-4-boratricyclo[6.1.1.02,6]decane
CAS No.:230299-05-5
Molecular Formula:C₂₀H₃₂B₂O₄
Molecular Weight:358.094
Hs Code.:2905399590
European Community (EC) Number:673-659-0,673-660-6
Mol file:230299-05-5.mol

Synonyms:230299-05-5;230299-17-9;MFCD02683578;MFCD27664803;CID 11970270;SY038439;SY038501;FT-0644068;FT-0644070;A878356;(1S,2S,6R,8S)-2,9,9-trimethyl-4-[(1S,2S,6R,8S)-2,9,9-trimethyl-3,5-dioxa-4-boratricyclo[6.1.1.0^{2,6]decan-4-yl]-3,5-dioxa-4-boratricyclo[6.1.1.0^{2,6]decane;(2S,2'S,6R,6'R)-6,6',9,9,9',9'-Hexamethyl-4,4'-bi(3,5-dioxa-4-boratricyclo[6.1.1.02,6]decane);(3aR,3 inverted exclamation mark aR,4R,4 inverted exclamation mark R,6R,6 inverted exclamation mark R,7aS,7 inverted exclamation mark aS)-3a,3 inverted exclamation mark a,5,5,5 inverted exclamation mark ,5 inverted exclamation mark -Hexamethyldodecahydro-2,2 inverted exclamation mark -bi[4,6-methanobenzo[d][1,3,2]dioxaborole];(3aS,3 inverted exclamation mark aS,4S,4 inverted exclamation mark S,6S,6 inverted exclamation mark S,7aR,7 inverted exclamation mark aR)-3a,3 inverted exclamation mark a,5,5,5 inverted exclamation mark ,5 inverted exclamation mark -Hexamethyldodecahydro-2,2 inverted exclamation mark -bi[4,6-methanobenzo[d][1,3,2]dioxaborole]

Suppliers and Price of 2,9,9-Trimethyl-4-(2,9,9-trimethyl-3,5-dioxa-4-boratricyclo[6.1.1.02,6]decan-4-yl)-3,5-dioxa-4-boratricyclo[6.1.1.02,6]decane

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

TRC
Bis[(+)-pinanediolato]diboron
100mg
$ 45.00

SynQuest Laboratories
Bis[(+)-pinanediolato]diboron
1 g
$ 72.00

SynQuest Laboratories
Bis[(+)-pinanediolato]diboron
5 g
$ 280.00

Sigma-Aldrich
BIS[(-)PINANEDIOLATO]DIBORON Aldrich
500mg
$ 144.00

Crysdot
(3aS,3'aS,4S,4'S,6S,6'S,7aR,7'aR)-3a,3'a,5,5,5',5'-Hexamethyldodecahydro-2,2'-bi[4,6-methanobenzo[d][1,3,2]dioxaborole] 95+%
10g
$ 463.00

ChemSupplyAustralia
Bis[(-)pinanediolato]diboron, 99%
500 mg
$ 85.80

ChemScene
(3aS,3′aS,4S,4′S,6S,6′S,7aR,7′aR)-Dodecahydro-3a,3′a,5,5,5′,5′-hexamethyl-2,2′-bi-4,6-methano-1,3,2-benzodioxaborole ≥98.0%
1g
$ 53.00

ChemScene
(3aS,3′aS,4S,4′S,6S,6′S,7aR,7′aR)-Dodecahydro-3a,3′a,5,5,5′,5′-hexamethyl-2,2′-bi-4,6-methano-1,3,2-benzodioxaborole ≥98.0%
5g
$ 117.00

ChemScene
(3aS,3′aS,4S,4′S,6S,6′S,7aR,7′aR)-Dodecahydro-3a,3′a,5,5,5′,5′-hexamethyl-2,2′-bi-4,6-methano-1,3,2-benzodioxaborole ≥98.0%
10g
$ 227.00

Biosynth Carbosynth
(+)-Bis(pinanediolato)diboron
10 g
$ 300.00

Total 33 raw suppliers

Chemical Property of 2,9,9-Trimethyl-4-(2,9,9-trimethyl-3,5-dioxa-4-boratricyclo[6.1.1.02,6]decan-4-yl)-3,5-dioxa-4-boratricyclo[6.1.1.02,6]decane

Chemical Property:

Vapor Pressure:4.56E-05mmHg at 25°C
Melting Point:147-151 °C(lit.)
Refractive Index:1.516
Boiling Point:360.606 °C at 760 mmHg
Flash Point:171.888 °C
PSA：36.92000
Density:1.126 g/cm³
LogP:3.52140
Storage Temp.:2-8°C
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:1
Exact Mass:358.2486698
Heavy Atom Count:26
Complexity:612

Purity/Quality:

99% ^*data from raw suppliers

Bis[(+)-pinanediolato]diboron ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:
Statements: 36/37/38
Safety Statements: 26-37-60

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:B1(OC2CC3CC(C3(C)C)C2(O1)C)B4OC5CC6CC(C6(C)C)C5(O4)C

Technology Process of 2,9,9-Trimethyl-4-(2,9,9-trimethyl-3,5-dioxa-4-boratricyclo[6.1.1.02,6]decan-4-yl)-3,5-dioxa-4-boratricyclo[6.1.1.02,6]decane

There total 1 articles about 2,9,9-Trimethyl-4-(2,9,9-trimethyl-3,5-dioxa-4-boratricyclo[6.1.1.02,6]decan-4-yl)-3,5-dioxa-4-boratricyclo[6.1.1.02,6]decane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 13675-18-8
tetrahydroxydiboron

: 22422-34-0
(1R,2R,3S,5R)-2,3-pinane diol

: 230299-05-5,230299-17-9
bis((-)pinanediolato)diboron

Guidance literature:: In tetrahydrofuran; at 70 ℃; for 3h; Molecular sieve;
DOI:10.1021/jacs.0c04558

Reference yield: 93.0%

: 230299-05-5,230299-17-9
bis-(+)-pinanediolato diboron

: 143825-84-7
4,4,5,5-tetramethyl-2-(1-phenylvinyl)-1,3,2-dioxaborolane

: (3aS,7aR)-3a,5,5-trimethyl-2-(1-phenylvinyl)hexahydro-4,6-methanobenzo[d][1,3,2]dioxaborole

Guidance literature:: In methanol; at 90 ℃; for 16h; Schlenk technique; Inert atmosphere;
DOI:10.1039/d1cc05815k

Reference yield: 90.0%

: 507469-89-8
(R)-(-)-N-(4-chlorobenzylidene)-2-methylpropane-2-sulfinamide

: 230299-05-5,230299-17-9
bis-(+)-pinanediolato diboron

: 1536530-76-3
C₂₁H₃₁BClNO₃S

Guidance literature:: With 2,5,6,7-tetrahydro-2-phenyl-3H-pyrrolo[2,1-c]-1,2,4-triazol-3-ylidenium chloride; caesium carbonate; copper(l) chloride; at 20 ℃; for 12h;
DOI:10.1039/c4ra02229g