[R-(R*,S*)]-[3-Azido-2-hydroxy-1-(phenylmethyl) propyl]carbamic acid, 1,1-dimethylethyl ester

Base Information

• Chemical Name: [R-(R*,S*)]-[3-Azido-2-hydroxy-1-(phenylmethyl) propyl]carbamic acid, 1,1-dimethylethyl ester
• CAS No.: 162536-72-3
• Molecular Formula: C₁₅H₂₂N₄O₃
• Molecular Weight: 306.365

Synonyms:[R-(R*,S*)]-[3-Azido-2-hydroxy-1-(phenylmethyl) propyl]carbamic acid, 1,1-dimethylethyl ester

Chemical Property of [R-(R*,S*)]-[3-Azido-2-hydroxy-1-(phenylmethyl) propyl]carbamic acid, 1,1-dimethylethyl ester

Chemical Property:

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Technology Process of [R-(R*,S*)]-[3-Azido-2-hydroxy-1-(phenylmethyl) propyl]carbamic acid, 1,1-dimethylethyl ester

There total 8 articles about [R-(R*,S*)]-[3-Azido-2-hydroxy-1-(phenylmethyl) propyl]carbamic acid, 1,1-dimethylethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

(1-oxiranyl-2-phenylethyl)carbamic acid tert-butyl ester (98760-08-8,98818-34-9,98818-35-0,103127-56-6,98737-29-2) → [R-(R*,S*)]-[3-Azido-2-hydroxy-1-(phenylmethyl) propyl]carbamic acid, 1,1-dimethylethyl ester (162536-72-3)

Guidance literature:

With sodium azide; ammonium chloride; In ethanol; water; at 80 ℃; for 12h;

Reference yield: 90.0%

[S-(R*,R*)]-(1-oxiranyl-2-phenylethyl)-carbamic acid 1,1-dimethylethyl ester (103127-56-6) → [R-(R*,S*)]-[3-Azido-2-hydroxy-1-(phenylmethyl) propyl]carbamic acid, 1,1-dimethylethyl ester (162536-72-3)

Guidance literature:

With sodium azide; In N,N-dimethyl-formamide; at 80 ℃; for 12h;

Reference yield:

(2R,3S)-3-[N-(tert-butyloxycarbonyl)amino]-1,2-epoxy-4-phenylbutane (98760-08-8) → [R-(R*,S*)]-[3-Azido-2-hydroxy-1-(phenylmethyl) propyl]carbamic acid, 1,1-dimethylethyl ester (162536-72-3)

Guidance literature:

With lithium azide; ammonium chloride; In ethanol; water; at 75 ℃; for 2h;

upstream raw materials:

(1-oxiranyl-2-phenylethyl)carbamic acid tert-butyl ester

N-tert-butoxycarbonyl-L-phenylalanine

(3S)-tert-butyl 1-benzyl-3-diazo-2-oxopropylcarbamate

Boc-Phe-O-COO-isoBu

Downstream raw materials:

N-[(1S,2R)-3-azido-1-benzyl-2-hydroxypropyl]-3-[(benzylsulfonyl)(methyl)amino]benzamide

(4S,5R)-5-azidomethyl-4-benzyl-3-methyl-oxazolidin-2-one

((1S,2R)-3-Amino-1-benzyl-2-methoxy-propyl)-carbamic acid tert-butyl ester

{(1S,2R)-3-[(Benzo[1,3]dioxole-5-sulfonyl)-(4-dibenzylamino-2,2-dimethyl-butyl)-amino]-1-benzyl-2-hydroxy-propyl}-carbamic acid (3R,3aS,6aR)-(hexahydro-furo[2,3-b]furan-3-yl) ester

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