1,12-bis-(3'-benzoyloxypropyl)-2,11-dihydroxy-4,6,7,9-tetramethoxy-3,10-perylenequinone

Base Information

Chemical Name:1,12-bis-(3'-benzoyloxypropyl)-2,11-dihydroxy-4,6,7,9-tetramethoxy-3,10-perylenequinone
CAS No.:329762-60-9
Molecular Formula:C₄₄H₃₈O₁₂
Molecular Weight:758.779
Hs Code.:

Synonyms:1,12-bis-(3'-benzoyloxypropyl)-2,11-dihydroxy-4,6,7,9-tetramethoxy-3,10-perylenequinone

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Chemical Property of 1,12-bis-(3'-benzoyloxypropyl)-2,11-dihydroxy-4,6,7,9-tetramethoxy-3,10-perylenequinone

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Technology Process of 1,12-bis-(3'-benzoyloxypropyl)-2,11-dihydroxy-4,6,7,9-tetramethoxy-3,10-perylenequinone

There total 4 articles about 1,12-bis-(3'-benzoyloxypropyl)-2,11-dihydroxy-4,6,7,9-tetramethoxy-3,10-perylenequinone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 329762-59-6
3-(3'-benzoyloxypropyl)-6,8-dimethoxy-1,2-naphthoquinone

: 329762-60-9
1,12-bis-(3'-benzoyloxypropyl)-2,11-dihydroxy-4,6,7,9-tetramethoxy-3,10-perylenequinone

Guidance literature:: With trifluoroacetic acid; In acetonitrile; at 20 ℃; for 2h;
DOI:10.1021/jo0014663

Reference yield:

: 329762-57-4
2-tert-butylamino-3-(3'-hydroxypropyl)-1,6,8-trimethoxynaphthalene

: 329762-60-9
1,12-bis-(3'-benzoyloxypropyl)-2,11-dihydroxy-4,6,7,9-tetramethoxy-3,10-perylenequinone

Guidance literature:: Multi-step reaction with 3 steps

1: 78 percent / tetrabutylammonium hydrogen sulfate; NaOH / CH₂Cl₂; H₂O / 24 h / 20 °C

2: 98 percent / DDQ; NaOH / CH₂Cl₂; H₂O / 1 h / 20 °C

3: 87 percent / Fe₃Cl; TFA / acetonitrile / 2 h / 20 °C

With sodium hydroxide; tetra(n-butyl)ammonium hydrogensulfate; trifluoroacetic acid; 2,3-dicyano-5,6-dichloro-p-benzoquinone; In dichloromethane; water; acetonitrile;
DOI:10.1021/jo0014663

Reference yield:

: 329762-58-5
3-(3'-benzoyloxypropyl)-2-tert-butylamino-1,6,8-trimethoxynaphthalene

: 329762-60-9
1,12-bis-(3'-benzoyloxypropyl)-2,11-dihydroxy-4,6,7,9-tetramethoxy-3,10-perylenequinone

Guidance literature:: Multi-step reaction with 2 steps

1: 98 percent / DDQ; NaOH / CH₂Cl₂; H₂O / 1 h / 20 °C

2: 87 percent / Fe₃Cl; TFA / acetonitrile / 2 h / 20 °C

With sodium hydroxide; trifluoroacetic acid; 2,3-dicyano-5,6-dichloro-p-benzoquinone; In dichloromethane; water; acetonitrile;
DOI:10.1021/jo0014663