C₄₈H₄₆O₁₂Si

Base Information

Chemical Name:C₄₈H₄₆O₁₂Si
CAS No.:1616873-41-6
Molecular Formula:C₄₈H₄₆O₁₂Si
Molecular Weight:842.972
Hs Code.:

C<sub>48</sub>H<sub>46</sub>O<sub>12</sub>Si

Synonyms:C₄₈H₄₆O₁₂Si

Suppliers and Price of C₄₈H₄₆O₁₂Si

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of C₄₈H₄₆O₁₂Si

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of C₄₈H₄₆O₁₂Si

There total 28 articles about C₄₈H₄₆O₁₂Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 1616873-24-5
C₃₆H₂₃BrO₉

: 1616873-39-2
C₂₄H₅₀O₃SiSn

: 1616873-41-6
C₄₈H₄₆O₁₂Si

Guidance literature:: With bis(tri-t-butylphosphine)palladium⁽⁰⁾; In toluene; at 80 ℃; for 0.25h; Inert atmosphere;
DOI:10.1002/chem.201402254

Reference yield:

: 1616873-05-2
C₂₅H₂₉ClO₈

: 1616873-41-6
C₄₈H₄₆O₁₂Si

Guidance literature:: Multi-step reaction with 11 steps

1.1: hydrogenchloride; water / methanol; tetrahydrofuran / 16 h / 50 °C

2.1: toluene-4-sulfonic acid / acetone / 0.33 h / Inert atmosphere

2.2: 0.33 h

3.1: triethylamine; dmap / dichloromethane / 2 h / 0 °C / Inert atmosphere

4.1: hydrogenchloride; water / methanol; tetrahydrofuran / 16 h / 50 °C

5.1: methanesulfonyl chloride; N-ethyl-N,N-diisopropylamine / dichloromethane / 0 °C / Inert atmosphere

5.2: 1 h / 0 °C / Inert atmosphere

6.1: ammonium cerium (IV) nitrate / water; ethyl acetate; acetonitrile / 1.25 h / 0 °C

7.1: toluene / 12 h / 100 °C / Schlenk technique; Inert atmosphere

8.1: Jones reagent; potassium fluoride / acetone / 45 h / 0 °C / Inert atmosphere

9.1: triethylamine / 0.17 h / Inert atmosphere

10.1: dmap; pyridine / dichloromethane / 16 h / 0 - 20 °C / Inert atmosphere

11.1: bis(tri-t-butylphosphine)palladium⁽⁰⁾ / toluene / 0.25 h / 80 °C / Inert atmosphere

With pyridine; hydrogenchloride; dmap; potassium fluoride; Jones reagent; ammonium cerium (IV) nitrate; bis(tri-t-butylphosphine)palladium⁽⁰⁾; water; toluene-4-sulfonic acid; methanesulfonyl chloride; triethylamine; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; methanol; dichloromethane; water; ethyl acetate; acetone; toluene; acetonitrile; 7.1: |Diels-Alder Cycloaddition / 11.1: |Stille Cross Coupling;
DOI:10.1002/chem.201402254

Reference yield:

: C₂₅H₃₃ClO₉

: 1616873-41-6
C₄₈H₄₆O₁₂Si

Guidance literature:: Multi-step reaction with 13 steps

1.1: 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione / ethyl acetate / 20 h / 65 °C / Inert atmosphere

2.1: sodium acetate; acetic acid / 12 h / 80 °C / Inert atmosphere

3.1: hydrogenchloride; water / methanol; tetrahydrofuran / 16 h / 50 °C

4.1: toluene-4-sulfonic acid / acetone / 0.33 h / Inert atmosphere

4.2: 0.33 h

5.1: triethylamine; dmap / dichloromethane / 2 h / 0 °C / Inert atmosphere

6.1: hydrogenchloride; water / methanol; tetrahydrofuran / 16 h / 50 °C

7.1: methanesulfonyl chloride; N-ethyl-N,N-diisopropylamine / dichloromethane / 0 °C / Inert atmosphere

7.2: 1 h / 0 °C / Inert atmosphere

8.1: ammonium cerium (IV) nitrate / water; ethyl acetate; acetonitrile / 1.25 h / 0 °C

9.1: toluene / 12 h / 100 °C / Schlenk technique; Inert atmosphere

10.1: Jones reagent; potassium fluoride / acetone / 45 h / 0 °C / Inert atmosphere

11.1: triethylamine / 0.17 h / Inert atmosphere

12.1: dmap; pyridine / dichloromethane / 16 h / 0 - 20 °C / Inert atmosphere

13.1: bis(tri-t-butylphosphine)palladium⁽⁰⁾ / toluene / 0.25 h / 80 °C / Inert atmosphere

With pyridine; hydrogenchloride; dmap; potassium fluoride; Jones reagent; ammonium cerium (IV) nitrate; bis(tri-t-butylphosphine)palladium⁽⁰⁾; water; sodium acetate; toluene-4-sulfonic acid; acetic acid; methanesulfonyl chloride; triethylamine; N-ethyl-N,N-diisopropylamine; 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione; In tetrahydrofuran; methanol; dichloromethane; water; ethyl acetate; acetone; toluene; acetonitrile; 9.1: |Diels-Alder Cycloaddition / 13.1: |Stille Cross Coupling;
DOI:10.1002/chem.201402254