p-methoxyphenyl 4,6-di-O-acetyl-2,3-di-O-benzyl-α-D-glucopyranosyl-(1→2)-6-O-benzyl-3-O-benzoyl-4-O-(2,3,4-tri-O-acetyl-α-L-rhamnopyranosyl)-β-D-glucopyranoside

Base Information

Chemical Name:p-methoxyphenyl 4,6-di-O-acetyl-2,3-di-O-benzyl-α-D-glucopyranosyl-(1→2)-6-O-benzyl-3-O-benzoyl-4-O-(2,3,4-tri-O-acetyl-α-L-rhamnopyranosyl)-β-D-glucopyranoside
CAS No.:1453195-48-6
Molecular Formula:C₆₃H₇₀O₂₂
Molecular Weight:1179.24
Hs Code.:

p-methoxyphenyl 4,6-di-O-acetyl-2,3-di-O-benzyl-α-D-glucopyranosyl-(1→2)-6-O-benzyl-3-O-benzoyl-4-O-(2,3,4-tri-O-acetyl-α-L-rhamnopyranosyl)-β-D-glucopyranoside

Synonyms:p-methoxyphenyl 4,6-di-O-acetyl-2,3-di-O-benzyl-α-D-glucopyranosyl-(1→2)-6-O-benzyl-3-O-benzoyl-4-O-(2,3,4-tri-O-acetyl-α-L-rhamnopyranosyl)-β-D-glucopyranoside

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Chemical Property of p-methoxyphenyl 4,6-di-O-acetyl-2,3-di-O-benzyl-α-D-glucopyranosyl-(1→2)-6-O-benzyl-3-O-benzoyl-4-O-(2,3,4-tri-O-acetyl-α-L-rhamnopyranosyl)-β-D-glucopyranoside

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Technology Process of p-methoxyphenyl 4,6-di-O-acetyl-2,3-di-O-benzyl-α-D-glucopyranosyl-(1→2)-6-O-benzyl-3-O-benzoyl-4-O-(2,3,4-tri-O-acetyl-α-L-rhamnopyranosyl)-β-D-glucopyranoside

There total 1 articles about p-methoxyphenyl 4,6-di-O-acetyl-2,3-di-O-benzyl-α-D-glucopyranosyl-(1→2)-6-O-benzyl-3-O-benzoyl-4-O-(2,3,4-tri-O-acetyl-α-L-rhamnopyranosyl)-β-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 1453195-47-5
p-methoxyphenyl 4,6-di-O-acetyl-2,3-di-O-benzyl-α-D-glucopyranosyl-(1→2)-6-O-benzyl-3-O-benzoyl-β-D-glucopyranoside

: 620951-70-4
p-tolyl 2,3,4-tri-O-acetyl-1-thio-α-L-rhamnopyranoside

: 1453195-48-6
p-methoxyphenyl 4,6-di-O-acetyl-2,3-di-O-benzyl-α-D-glucopyranosyl-(1→2)-6-O-benzyl-3-O-benzoyl-4-O-(2,3,4-tri-O-acetyl-α-L-rhamnopyranosyl)-β-D-glucopyranoside

Guidance literature:: p-methoxyphenyl 4,6-di-O-acetyl-2,3-di-O-benzyl-α-D-glucopyranosyl-(1→2)-6-O-benzyl-3-O-benzoyl-β-D-glucopyranoside; p-tolyl 2,3,4-tri-O-acetyl-1-thio-α-L-rhamnopyranoside; In dichloromethane; at 0 ℃; for 0.5h; Molecular sieve; Inert atmosphere;

With N-iodo-succinimide; sulfuric acid; silica gel; In dichloromethane; for 0.5h; Molecular sieve; Inert atmosphere;
DOI:10.1016/j.carres.2013.06.009

Reference yield: 81.0%

: 1453195-48-6
p-methoxyphenyl 4,6-di-O-acetyl-2,3-di-O-benzyl-α-D-glucopyranosyl-(1→2)-6-O-benzyl-3-O-benzoyl-4-O-(2,3,4-tri-O-acetyl-α-L-rhamnopyranosyl)-β-D-glucopyranoside

: 1453195-49-7
p-methoxyphenyl 4,6-di-O-acetyl-β-D-glucopyranosyl-(1→2)-3-O-benzoyl-4-O-(2,3,4-tri-O-acetyl-α-L-rhamnopyranosyl)-β-D-glucopyranoside

Guidance literature:: With palladium 10% on activated carbon; hydrogen; acetic anhydride; In methanol;
DOI:10.1016/j.carres.2013.06.009

Reference yield:

: 1453195-48-6
p-methoxyphenyl 4,6-di-O-acetyl-2,3-di-O-benzyl-α-D-glucopyranosyl-(1→2)-6-O-benzyl-3-O-benzoyl-4-O-(2,3,4-tri-O-acetyl-α-L-rhamnopyranosyl)-β-D-glucopyranoside

: 1453195-50-0
p-methoxyphenyl 4-O-(α-L-rhamnopyranosyl)-α-D-glucopyranosyl-(1→2)-β-D-glucopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1.1: acetic anhydride; palladium 10% on activated carbon; hydrogen / methanol

2.1: sodium methylate / methanol / 12 h / 20 °C

2.2: DOWEX 50W H⁺resin

With palladium 10% on activated carbon; hydrogen; sodium methylate; acetic anhydride; In methanol;
DOI:10.1016/j.carres.2013.06.009