all-cis-1,2,3-triphenyl-2,3-dihydro-1H-cyclopenta[l]phenantrene

Base Information

Chemical Name:all-cis-1,2,3-triphenyl-2,3-dihydro-1H-cyclopenta[l]phenantrene
CAS No.:1257635-97-4
Molecular Formula:C₃₅H₂₆
Molecular Weight:446.591
Hs Code.:

Synonyms:all-cis-1,2,3-triphenyl-2,3-dihydro-1H-cyclopenta[l]phenantrene

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of all-cis-1,2,3-triphenyl-2,3-dihydro-1H-cyclopenta[l]phenantrene

Chemical Property:

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Technology Process of all-cis-1,2,3-triphenyl-2,3-dihydro-1H-cyclopenta[l]phenantrene

There total 6 articles about all-cis-1,2,3-triphenyl-2,3-dihydro-1H-cyclopenta[l]phenantrene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.0%

: (3S*,4R*,5R*)-1,2,3,4,5-pentaphenylcyclopentene

: 2519-10-0
1,2,3,4,5-pentaphenylcyclopentadiene

: 1257635-97-4
all-cis-1,2,3-triphenyl-2,3-dihydro-1H-cyclopenta[l]phenantrene

Guidance literature:: With air; In toluene; for 33h; UV-irradiation;
DOI:10.1002/ejoc.201000821

Reference yield:

: 2137-74-8
1,2,3,4,5-pentaphenylcyclopenta-2,4-dien-1-ol

: 1257635-97-4
all-cis-1,2,3-triphenyl-2,3-dihydro-1H-cyclopenta[l]phenantrene

Guidance literature:: Multi-step reaction with 4 steps

1: 10% palladium on activated carbon; hydrogen / methanol; ethyl acetate / 48 h / 2250.23 Torr

2: iodine / methanol / 24 h / Inert atmosphere; UV-irradiation

3: 10% palladium on activated carbon; hydrogen / chloroform; ethyl acetate / 168 h / 2250.23 Torr

4: iodine / methanol / 16 h / Inert atmosphere; UV-irradiation

With 10% palladium on activated carbon; hydrogen; iodine; In methanol; chloroform; ethyl acetate;
DOI:10.1002/ejoc.201000821

Reference yield:

: 1257635-94-1
(1r*,2R*,5S*)-1,2,3,4,5-pentaphenylcyclopent-3-enol

: 1257635-97-4
all-cis-1,2,3-triphenyl-2,3-dihydro-1H-cyclopenta[l]phenantrene

Guidance literature:: Multi-step reaction with 4 steps

1: iodine / methanol / 24 h / Inert atmosphere; UV-irradiation

2: sodium hydroxide / water / 0.5 h / Heating

3: hydrogen / methanol; ethyl acetate / 48 h / 2250.23 Torr

4: iodine / methanol / 16 h / Inert atmosphere; UV-irradiation

With hydrogen; iodine; sodium hydroxide; In methanol; water; ethyl acetate;
DOI:10.1002/ejoc.201000821