(R(Fc))-(α-p-methoxyphenyl)-1,3-benzodithiol-2-ylferrocenylvinyl

Base Information

Chemical Name:(R(Fc))-(α-p-methoxyphenyl)-1,3-benzodithiol-2-ylferrocenylvinyl
CAS No.:721944-89-4
Molecular Formula:C₂₅H₂₀FeOS₂
Molecular Weight:456.412
Hs Code.:

Synonyms:(R(Fc))-(α-p-methoxyphenyl)-1,3-benzodithiol-2-ylferrocenylvinyl

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (R(Fc))-(α-p-methoxyphenyl)-1,3-benzodithiol-2-ylferrocenylvinyl

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Technology Process of (R(Fc))-(α-p-methoxyphenyl)-1,3-benzodithiol-2-ylferrocenylvinyl

There total 1 articles about (R(Fc))-(α-p-methoxyphenyl)-1,3-benzodithiol-2-ylferrocenylvinyl which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 62217-21-4
diethyl benzo[d][1,3]dithiol-2-yl-phosphonate

: 344914-05-2,63397-85-3
(R(Fc))-(α-p-methoxyphenyl)ferrocenecarboxaldehyde

: 721944-89-4
(R(Fc))-(α-p-methoxyphenyl)-1,3-benzodithiol-2-ylferrocenylvinyl

Guidance literature:: With potassium tert-butylate; In tetrahydrofuran; under Ar; THF added to mixt. of Fe-complex and phosphonate in Schlenk tube, cooled to 0°C, soln. of t-BuOK in THF slowly added, mixt. warmed to room temp., stirred overnight; quenched with water at 0°C, extd. with CH2Cl2, extract dried overMgSO4, filtered, filtrate evapd., flash chromy. (silica gel, Et2O/CH2Cl 2 (1/1));
DOI:10.1039/b300397n