acetic acid 10-(3,5-dihydroxy-phenoxymethyl)-anthracen-9-ylmethyl ester

Base Information

• Chemical Name: acetic acid 10-(3,5-dihydroxy-phenoxymethyl)-anthracen-9-ylmethyl ester
• CAS No.: 885481-25-4
• Molecular Formula: C₂₄H₂₀O₅
• Molecular Weight: 388.42
• Mol file: 885481-25-4.mol

Synonyms:acetic acid 10-(3,5-dihydroxy-phenoxymethyl)-anthracen-9-ylmethyl ester

Chemical Property of acetic acid 10-(3,5-dihydroxy-phenoxymethyl)-anthracen-9-ylmethyl ester

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of acetic acid 10-(3,5-dihydroxy-phenoxymethyl)-anthracen-9-ylmethyl ester

There total 5 articles about acetic acid 10-(3,5-dihydroxy-phenoxymethyl)-anthracen-9-ylmethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

C38H28O7 (885481-24-3) → acetic acid 10-(3,5-dihydroxy-phenoxymethyl)-anthracen-9-ylmethyl ester (885481-25-4)

Guidance literature:

With N-butylamine; In tetrahydrofuran; for 18h; Heating;

DOI:10.1016/j.tet.2006.01.024

Reference yield:

9-acetoxymethyl-10-bromomethylanthracene (713143-47-6) → acetic acid 10-(3,5-dihydroxy-phenoxymethyl)-anthracen-9-ylmethyl ester (885481-25-4)

Guidance literature:

Multi-step reaction with 2 steps

1: 90 percent / potassium carbonate; 18-crown-6 / dimethylformamide / 4 h / 55 °C

2: 81 percent / n-butylamine / tetrahydrofuran / 18 h / Heating

With 18-crown-6 ether; potassium carbonate; N-butylamine; In tetrahydrofuran; N,N-dimethyl-formamide;

DOI:10.1016/j.tet.2006.01.024

Reference yield:

1,3,5-Tribenzoyloxybenzene (7510-54-5) → acetic acid 10-(3,5-dihydroxy-phenoxymethyl)-anthracen-9-ylmethyl ester (885481-25-4)

Guidance literature:

Multi-step reaction with 3 steps

1: 79 percent / cesium carbonate / 1,2-dimethoxy-ethane / 18 h / Heating

2: 90 percent / potassium carbonate; 18-crown-6 / dimethylformamide / 4 h / 55 °C

3: 81 percent / n-butylamine / tetrahydrofuran / 18 h / Heating

With 18-crown-6 ether; potassium carbonate; caesium carbonate; N-butylamine; In tetrahydrofuran; 1,2-dimethoxyethane; N,N-dimethyl-formamide;

DOI:10.1016/j.tet.2006.01.024

upstream raw materials:

C₃₈H₂₈O₇

9-acetoxymethyl-10-bromomethylanthracene

9-acetoxymethyl-10-methylanthracene

1,3,5-Tribenzoyloxybenzene